1H-Isoindole, 2,3-dihydro-1,1,3,3-tetraMethyl-

Base Information

• Chemical Name: 1H-Isoindole, 2,3-dihydro-1,1,3,3-tetraMethyl-
• CAS No.: 82894-84-6
• Molecular Formula: C12H17N
• Molecular Weight: 175.274
• Hs Code.: 2933990090
• Mol file: 82894-84-6.mol

Synonyms:1H-Isoindole, 2,3-dihydro-1,1,3,3-tetraMethyl-;1,1,3,3-TetraMethylisoindoline

Chemical Property of 1H-Isoindole, 2,3-dihydro-1,1,3,3-tetraMethyl-

Chemical Property:

• PSA: 12.03000
• LogP: 3.08880

Purity/Quality:

99%+ ^*data from raw suppliers

1,1,3,3-Tetramethylisoindoline 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Isoindole, 2,3-dihydro-1,1,3,3-tetraMethyl-

There total 7 articles about 1H-Isoindole, 2,3-dihydro-1,1,3,3-tetraMethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-bromo-1,1,3,3-tetramethylisoindoline (221368-73-6) → 1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindole (82894-84-6)

Guidance literature:

With sodium tungstate; dihydrogen peroxide; sodium hydrogencarbonate; In methanol;

Reference yield: 96.0%

2-benzyl-1,1,3,3-tetramethylisoindoline (82894-83-5) → 1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindole (82894-84-6)

Guidance literature:

With hydrogen; palladium on activated charcoal; In acetic acid;

DOI:10.1016/S0040-4039(00)87091-4

Reference yield: 45.8%

1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindol-2-yloxoyl radical (80037-90-7) + thiophenol (108-98-5) → 1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindole (82894-84-6) + diphenyldisulfane (882-33-7) + 2-(benzenesulfinyl)-1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindole + 1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindolinium benzenesulfinate

Guidance literature:

In benzene; at 60 ℃; for 0.666667h; Further Variations:; Temperatures; Product distribution;

DOI:10.1071/CH01100

upstream raw materials:

2-benzyl-1,1,3,3-tetramethylisoindoline

α,α,α',α'-tetramethyldipropargylamine

acetylene

2-bromo-1,1,3,3-tetramethylisoindoline

Downstream raw materials:

2-methoxy-1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindole

2-(2-tert-butoxy-1-phenylethoxy)-1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindole

N-benzoyl-1,1,3,3-tetramethyl-5-nitroisoindoline

N-benzoyl-1,1,3,3-tetramethylisoindoline

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