Technology Process of Carbamic acid, (2-benzoylphenyl)-, 1,1-dimethylethyl ester (9CI)
There total 3 articles about Carbamic acid, (2-benzoylphenyl)-, 1,1-dimethylethyl ester (9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutylammonium triphenyldifluorosilicate;
In
toluene;
at 50 ℃;
for 16h;
DOI:10.1021/ol902568x
- Guidance literature:
-
N-(t-butoxycarbonyl)-4-chloroaniline;
With
tert.-butyl lithium;
In
tetrahydrofuran; pentane;
at -78 - -20 ℃;
for 2.25h;
pyridine-2-carbaldehyde;
at -78 ℃;
for 2h;
With
manganese(IV) oxide;
In
chloroform;
for 18h;
- Guidance literature:
-
di-tert-butyl dicarbonate; (2-aminophenyl)(phenyl)methanone;
With
dmap;
at 65 - 70 ℃;
for 2h;
With
hydrazine hydrate;
In
ethanol;
at 20 - 70 ℃;
DOI:10.1039/c0ob01156h