Methyl 3-amino-2-hydroxy-5-methoxybenzoate 95+%

Base Information

• Chemical Name: Methyl 3-amino-2-hydroxy-5-methoxybenzoate 95+%
• CAS No.: 55008-18-9
• Molecular Formula: C9H11NO4
• Molecular Weight: 197.191
• Hs Code.: 2922509090
• Mol file: 55008-18-9.mol

Synonyms:Methyl 3-amino-2-hydroxy-5-methoxybenzoate 95+%;Methyl 3-amino-2-hydroxy-5-methoxybenzenecarboxylate;2-Amino-4-methoxy-6-(methoxycarbonyl)phenol;methyl 3-amino-2-hydroxy-5-methoxybenzoate

Chemical Property of Methyl 3-amino-2-hydroxy-5-methoxybenzoate 95+%

Chemical Property:

• PSA: 81.78000
• LogP: 1.35080

Purity/Quality:

97% ^*data from raw suppliers

Methyl 3-amino-2-hydroxy-5-methoxybenzoate 95.0% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 3-amino-2-hydroxy-5-methoxybenzoate 95+%

There total 2 articles about Methyl 3-amino-2-hydroxy-5-methoxybenzoate 95+% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 2-hydroxy-5-methoxy-3-nitrobenzoate (2888-09-7) → methyl 3-amino-2-hydroxy-5-methoxybenzoate (55008-18-9)

Guidance literature:

With hydrogen; platinum(IV) oxide; In tetrahydrofuran; methanol; for 1.5h;

Reference yield:

→ methyl 3-amino-2-hydroxy-5-methoxybenzoate (55008-18-9)

Guidance literature:

aus dem Ester (I) durch Reduktion mit Pd;

Reference yield:

4-(2-(o-tolyloxy)acetamido)benzoyl chloride (942216-39-9) + methyl 3-amino-2-hydroxy-5-methoxybenzoate (55008-18-9) → methyl 2-hydroxy-5-methoxy-3-[(4-{[(2-methylphenoxy)acetyl]amino}benzoyl)amino]benzoate

Guidance literature:

4-(2-(o-tolyloxy)acetamido)benzoyl chloride; methyl 3-amino-2-hydroxy-5-methoxybenzoate; In 1,4-dioxane; dichloromethane; at 100 ℃; for 2h;

With sodium hydrogencarbonate; In 1,4-dioxane; dichloromethane; ethyl acetate;

upstream raw materials:

methyl 2-hydroxy-5-methoxy-3-nitrobenzoate

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