Methyl 2-hydroxy-5-methoxy-3-nitrobenzoate 95+%

Base Information

• Chemical Name: Methyl 2-hydroxy-5-methoxy-3-nitrobenzoate 95+%
• CAS No.: 2888-09-7
• Molecular Formula: C9H9NO6
• Molecular Weight: 227.174
• Hs Code.: 2918990090
• Mol file: 2888-09-7.mol

Synonyms:Methyl 2-hydroxy-5-methoxy-3-nitrobenzoate 95+%;Methyl 2-hydroxy-5-methoxy-3-nitrobenzenecarboxylate;4-Methoxy-2-(methoxycarbonyl)-6-nitrophenol

Chemical Property of Methyl 2-hydroxy-5-methoxy-3-nitrobenzoate 95+%

Chemical Property:

• Melting Point: 138-139 °C
• Boiling Point: 333.5±37.0 °C(Predicted)
• PKA: 7.07±0.38(Predicted)
• PSA: 101.58000
• Density: 1.405±0.06 g/cm3(Predicted)
• LogP: 1.61880

Purity/Quality:

97% ^*data from raw suppliers

Methyl2-hydroxy-5-methoxy-3-nitrobenzenecarboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 2-hydroxy-5-methoxy-3-nitrobenzoate 95+%

There total 3 articles about Methyl 2-hydroxy-5-methoxy-3-nitrobenzoate 95+% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

methyl 5-methoxy-2-hydroxybenzoate (2905-82-0) → methyl 2-hydroxy-5-methoxy-3-nitrobenzoate (2888-09-7)

Guidance literature:

With bismuth(III) nitrate; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1021/ja100579z

Reference yield:

methyl 5-methoxy-2-hydroxybenzoate (2905-82-0) + nitric acid (7697-37-2,78989-43-2) + acetic acid (64-19-7,77671-22-8) → methyl 2-hydroxy-5-methoxy-3-nitrobenzoate (2888-09-7)

Guidance literature:

Reference yield:

→ methyl 2-hydroxy-5-methoxy-3-nitrobenzoate (2888-09-7)

Guidance literature:

3-Nitro-5-methoxy-salicylsaeure, Me., H2SO4 o. HCl;

upstream raw materials:

methyl 5-methoxy-2-hydroxybenzoate

nitric acid

acetic acid

Downstream raw materials:

2-hydroxy-5-methoxy-3-nitrobenzoic acid

methyl 3-amino-2-hydroxy-5-methoxybenzoate

methyl 2,5-Dimethoxy-3-nitrobenzoate

2,2-dimethyl-1,3-dioxane-4,6-dione

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