1,2-Benzenedicarboxylic acid bis(trimethylsilyl) ester

Base Information

Chemical Name:1,2-Benzenedicarboxylic acid bis(trimethylsilyl) ester
CAS No.:2078-22-0
Molecular Formula:C14H22O4Si2
Molecular Weight:310.497
Hs Code.:
Mol file:2078-22-0.mol

Synonyms:1,2-Benzenedicarboxylic acid bis(trimethylsilyl);1,2-Benzenedicarboxylic acid bis(trimethylsilyl) ester;Phthalic acid bis(trimethylsilyl);Phthalic acid bis(trimethylsilyl) ester

Suppliers and Price of 1,2-Benzenedicarboxylic acid bis(trimethylsilyl) ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1,2-Benzenedicarboxylic acid bis(trimethylsilyl) ester

Chemical Property:

Boiling Point:114 - 115 °C (1 mmHg)
PSA：52.60000
LogP:3.67000

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,2-Benzenedicarboxylic acid bis(trimethylsilyl) ester

There total 1 articles about 1,2-Benzenedicarboxylic acid bis(trimethylsilyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 88-99-3,73607-73-5
benzene-1,2-dicarboxylic acid

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 2078-22-0
ortho-phthalic acid bis(trimethylsilyl) ester

Guidance literature:: With saccharin; at 125 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.10.114

Reference yield: 79.0%

: (η(5)-C5Me5)2ZrF2

: 2078-22-0
ortho-phthalic acid bis(trimethylsilyl) ester

: [(η(5)-C5Me5)ZrF(μ-F)(μ-OCO-o-C6H4COOSiMe3)]2

Guidance literature:: In hexane; N2-atmosphere; stirring equimolar amts. for 24 h; crystn. on concn.; elem. anal.;
DOI:10.1016/S0022-328X(96)06818-0

Reference yield: 73.0%

: (pentamethylcyclopentadienyl)titanium fluoride

: 2078-22-0
ortho-phthalic acid bis(trimethylsilyl) ester

: 205492-26-8
[(η(5)-C5Me5)TiF(μ-F)(μ-OCO-o-C6H4COOSiMe3)]2

Guidance literature:: In toluene; N2-atmosphere; stirring equimolar amts. for 24 h; solvent removal (vac.), extn. into CH2Cl2, concn., crystn. (-25°C), recrystn. (CH2Cl2); elem. anal.;
DOI:10.1016/S0022-328X(96)06818-0