2-Benzoyl-5-nitrobenzoic acid methyl ester

Base Information

• Chemical Name: 2-Benzoyl-5-nitrobenzoic acid methyl ester
• CAS No.: 42156-50-3
• Molecular Formula: C₁₅H₁₁NO₅
• Molecular Weight: 285.256
• Mol file: 42156-50-3.mol

Synonyms:2-Benzoyl-5-nitrobenzoic acid methyl ester

Chemical Property of 2-Benzoyl-5-nitrobenzoic acid methyl ester

Chemical Property:

• PSA: 89.19000
• LogP: 3.13560

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Benzoyl-5-nitrobenzoic acid methyl ester

There total 6 articles about 2-Benzoyl-5-nitrobenzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitrophthalic anhydride (5466-84-2) → 5-Nitro-o-benzoylbenzoesaeuremethylester (42156-50-3)

Guidance literature:

Multi-step reaction with 2 steps

1: AlCl₃

2: concentrated sulfuric acid

With aluminium trichloride; sulfuric acid;

DOI:10.1007/BF01558892

Reference yield:

4-nitro-phthalic acid-1-methyl ester (90072-77-8) → 4-Nitro-o-benzoylbenzoesaeuremethylester (42156-49-0) + 5-Nitro-o-benzoylbenzoesaeuremethylester (42156-50-3)

Guidance literature:

With phosphorus pentachloride; benzene; Behandeln des Reaktionsprodukts mit Benzol und AlCl₃;

DOI:10.1039/jr9520000553

Reference yield:

benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → 5-Nitro-o-benzoylbenzoesaeuremethylester (42156-50-3)

Guidance literature:

Multi-step reaction with 2 steps

1: AlCl₃

2: concentrated sulfuric acid

With aluminium trichloride; sulfuric acid;

DOI:10.1007/BF01558892

upstream raw materials:

methanol

2-benzoyl-5-nitro-benzoic acid

4-nitro-phthalic acid-1-methyl ester

methyl iodide