5H-Pyrrolo[2,3-b:5,4-c']dipyridine, 6,7,8,9-tetrahydro-, hydrochloride

Base Information

• Chemical Name: 5H-Pyrrolo[2,3-b:5,4-c']dipyridine, 6,7,8,9-tetrahydro-, hydrochloride
• CAS No.: 1354801-06-1
• Molecular Formula: C10H12ClN3
• Molecular Weight: 209.678
• Hs Code.: 2933990090
• Mol file: 1354801-06-1.mol

Synonyms:5H-Pyrrolo[2,3-b:5,4-c']dipyridine, 6,7,8,9-tetrahydro-, hydrochloride

Chemical Property of 5H-Pyrrolo[2,3-b:5,4-c']dipyridine, 6,7,8,9-tetrahydro-, hydrochloride

Chemical Property:

• PSA: 40.71000
• LogP: 2.33940
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

6,7,8,9-Tetrahydro-5H-pyrrolo[2,3-b:5,4-c']dipyridinehydrochloride 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5H-Pyrrolo[2,3-b:5,4-c']dipyridine, 6,7,8,9-tetrahydro-, hydrochloride

There total 4 articles about 5H-Pyrrolo[2,3-b:5,4-c']dipyridine, 6,7,8,9-tetrahydro-, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 2-(1H-pyrrolo[2,3-b]pyridin-3-yl)-ethylamine (4649-12-1) → 6,7,8,9-tetrahydro-5H-pyrido[4′,3′:4,5]pyrrolo[2,3-b]pyridine hydrochloride (1354801-06-1)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; ethanol; water; for 3h; Reflux;

Reference yield:

7-Azaindole (271-63-6) → 6,7,8,9-tetrahydro-5H-pyrido[4′,3′:4,5]pyrrolo[2,3-b]pyridine hydrochloride (1354801-06-1)

Guidance literature:

Multi-step reaction with 4 steps

1.1: water; butan-1-ol / 2.5 h / 120 °C

2.1: dimethyl sulfate / methanol / 0.33 h / 20 °C / Cooling with ice

2.2: 1.73 h / Cooling with ice

3.1: 20% palladium hydroxide-activated charcoal; hydrogen / ethanol / 16 h / 70 °C

4.1: hydrogenchloride / 1,4-dioxane; water; ethanol / 3 h / Reflux

With hydrogenchloride; 20% palladium hydroxide-activated charcoal; hydrogen; dimethyl sulfate; In 1,4-dioxane; methanol; ethanol; water; butan-1-ol;

Reference yield:

7-azagramine (5654-92-2) → 6,7,8,9-tetrahydro-5H-pyrido[4′,3′:4,5]pyrrolo[2,3-b]pyridine hydrochloride (1354801-06-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: dimethyl sulfate / methanol / 0.33 h / 20 °C / Cooling with ice

1.2: 1.73 h / Cooling with ice

2.1: 20% palladium hydroxide-activated charcoal; hydrogen / ethanol / 16 h / 70 °C

3.1: hydrogenchloride / 1,4-dioxane; water; ethanol / 3 h / Reflux

With hydrogenchloride; 20% palladium hydroxide-activated charcoal; hydrogen; dimethyl sulfate; In 1,4-dioxane; methanol; ethanol; water;

upstream raw materials:

7-Azaindole

formaldehyd

2-(1H-pyrrolo[2,3-b]pyridin-3-yl)-ethylamine

7-azagramine

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