Dodec-11-enylbenzene

Base Information

Chemical Name:Dodec-11-enylbenzene
CAS No.:256505-61-0
Molecular Formula:C₁₈H₂₈
Molecular Weight:244.42
Hs Code.:
DSSTox Substance ID:DTXSID101016047
Mol file:256505-61-0.mol

Synonyms:dodec-11-enylbenzene;12-Phenyldodecene;256505-61-0;(dodec-11-en-1-yl)benzene;USDGCWIXVQFFFE-UHFFFAOYSA-N;DODEC-11-EN-1-YLBENZENE;DTXSID101016047

Suppliers and Price of Dodec-11-enylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
12-PHENYLDODECENE 95.00%
5MG
$ 500.78

Total 2 raw suppliers

Chemical Property of Dodec-11-enylbenzene

Chemical Property:

Boiling Point:130°C / 3
XLogP3:8.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:11
Exact Mass:244.219100893
Heavy Atom Count:18
Complexity:177

Purity/Quality:

99% ^*data from raw suppliers

12-PHENYLDODECENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C=CCCCCCCCCCCC1=CC=CC=C1

Technology Process of Dodec-11-enylbenzene

There total 3 articles about Dodec-11-enylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 7766-50-9
1-undecen-11-ylbromide

: 6921-34-2
benzylmagnesium chloride

: 256505-61-0
dodec-11-en-1-ylbenzene

Guidance literature:: In tetrahydrofuran; for 96h;
DOI:10.1021/acs.orglett.5b01135

Reference yield: 45.0%

: 7766-50-9
1-undecen-11-ylbromide

: 5281-18-5
benzaldehyde, hydrazone

: 256505-61-0
dodec-11-en-1-ylbenzene

Guidance literature:: With tetrakis(pyridine)nickel dichloride; potassium tert-butylate; triphenylphosphine; In 1,4-dioxane; at 60 ℃; for 24h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.9b00649

Reference yield:

: 100-52-7
benzaldehyde

: 256505-61-0
dodec-11-en-1-ylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate

2: tetrakis(pyridine)nickel dichloride; triphenylphosphine; potassium tert-butylate / 1,4-dioxane / 24 h / 60 °C / Schlenk technique; Inert atmosphere

With tetrakis(pyridine)nickel dichloride; potassium tert-butylate; hydrazine hydrate; triphenylphosphine; In 1,4-dioxane;
DOI:10.1021/acs.joc.9b00649