METHYL 6-HYDROXYVERATRATE

Base Information

• Chemical Name: METHYL 6-HYDROXYVERATRATE
• CAS No.: 28373-21-9
• Molecular Formula: C10H12O5
• Molecular Weight: 212.202
• Mol file: 28373-21-9.mol

Synonyms:METHYL 6-HYDROXYVERATRATE

Chemical Property of METHYL 6-HYDROXYVERATRATE

Chemical Property:

• Vapor Pressure: 8.17E-05mmHg at 25°C
• Boiling Point: 331.3°C at 760 mmHg
• Flash Point: 128.4°C
• PSA: 64.99000
• Density: 1.221g/cm³
• LogP: 1.19600

Purity/Quality:

99% ^*data from raw suppliers

METHYL-6-HYDROXYVERATRATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of METHYL 6-HYDROXYVERATRATE

There total 14 articles about METHYL 6-HYDROXYVERATRATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.8%

2,4,5-trihydroxybenzoic acid (610-90-2) + methyl iodide (74-88-4) → 2-hydroxy-4,5-dimethoxybenzoic acid methyl ester (28373-21-9)

Guidance literature:

2,4,5-trihydroxybenzoic acid; With sodium hydroxide; In ethanol; for 0.5h;

methyl iodide; In ethanol; at 50 ℃; for 5h; Temperature; Solvent; Reagent/catalyst;

Reference yield:

asaronic acid (490-64-2) → 2-hydroxy-4,5-dimethoxybenzoic acid methyl ester (28373-21-9)

Guidance literature:

Multi-step reaction with 2 steps

1: BCl₃ / CH₂Cl₂

2: 79 percent / H₂SO₄ / Heating

With sulfuric acid; boron trichloride; In dichloromethane;

DOI:10.1016/j.bmcl.2006.07.075

Reference yield:

methyl 2-amino-4,5-dimethoxybenzoate (26759-46-6) → 2-hydroxy-4,5-dimethoxybenzoic acid methyl ester (28373-21-9)

Guidance literature:

With sulfuric acid; copper(II) sulfate;

DOI:10.1021/ja01264a076

upstream raw materials:

diazomethane

2-hydroxy-4,5-dimethoxybenzoic acid

methyl 2-amino-4,5-dimethoxybenzoate

2,2,2-trichloro-1-(2-hydroxy-4,5-dimethoxy-phenyl)-ethanone

Downstream raw materials:

2-hydroxy-4,5-dimethoxybenzoic acid

2-allyloxy-4,5-dimethoxy-benzoic acid methyl ester

2-(5-Iodo-3,6-dioxo-cyclohexa-1,4-dienyloxy)-4,5-dimethoxy-benzoic acid methyl ester

N-(3-{[2-(3,4-Dimethoxy-phenyl)-ethyl]-methyl-amino}-propyl)-2-hydroxy-4,5-dimethoxy-benzamide

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