2-Isopropyl-2-(3,4-dimethoxyphenyl)-5-[(formyl)methylamino]pentanenitrile

Base Information

Chemical Name:2-Isopropyl-2-(3,4-dimethoxyphenyl)-5-[(formyl)methylamino]pentanenitrile
CAS No.:42601-11-6
Molecular Formula:C18H26N2O3
Molecular Weight:318.416
Hs Code.:
Mol file:42601-11-6.mol

Synonyms:2-Isopropyl-2-(3,4-dimethoxyphenyl)-5-[(formyl)methylamino]pentanenitrile

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Isopropyl-2-(3,4-dimethoxyphenyl)-5-[(formyl)methylamino]pentanenitrile

Chemical Property:

PSA：62.56000
LogP:3.62548

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Isopropyl-2-(3,4-dimethoxyphenyl)-5-[(formyl)methylamino]pentanenitrile

There total 3 articles about 2-Isopropyl-2-(3,4-dimethoxyphenyl)-5-[(formyl)methylamino]pentanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93-17-4
3,4-dimethoxyphenylacetonitrile

: 42601-11-6
(dimethoxy-3,4 phenyl)-2 (N-methyl N-formyl amino-3 propyl)-2 isovaleronitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, RT, 5 h, 2.) RT, overnight

2: 1.) NaH / 1.) DMF, 80 deg C, 5 h, 2.) 80 deg C, 20 h

With sodium hydride;
DOI:10.1016/0223-5234(90)90119-N

Reference yield:

: 4172-04-7
N-methyl N-(chloro-3 propyl) formamide

: 20850-49-1
2-(3,4-dimethoxyphenyl)-3-methylbutyronitrile

: 42601-11-6
(dimethoxy-3,4 phenyl)-2 (N-methyl N-formyl amino-3 propyl)-2 isovaleronitrile

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, 80 deg C, 5 h, 2.) 80 deg C, 20 h;
DOI:10.1016/0223-5234(90)90119-N