4-[(benzyloxy)methyl]-1-(pyridin-4-yl)piperidine-4-carboxylic acid

Base Information

Chemical Name:4-[(benzyloxy)methyl]-1-(pyridin-4-yl)piperidine-4-carboxylic acid
CAS No.:1203600-34-3
Molecular Formula:C₁₉H₂₂N₂O₃
Molecular Weight:326.395
Hs Code.:
Mol file:1203600-34-3.mol

Synonyms:4-[(benzyloxy)methyl]-1-(pyridin-4-yl)piperidine-4-carboxylic acid

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Chemical Property of 4-[(benzyloxy)methyl]-1-(pyridin-4-yl)piperidine-4-carboxylic acid

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Technology Process of 4-[(benzyloxy)methyl]-1-(pyridin-4-yl)piperidine-4-carboxylic acid

There total 3 articles about 4-[(benzyloxy)methyl]-1-(pyridin-4-yl)piperidine-4-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1203600-35-4
C₂₁H₂₆N₂O₃

: 1203600-34-3
4-[(benzyloxy)methyl]-1-(pyridin-4-yl)piperidine-4-carboxylic acid

Guidance literature:: C₂₁H₂₆N₂O₃; With water; sodium hydroxide; In tetrahydrofuran; ethanol; at 50 ℃;

With hydrogenchloride; In water;

Reference yield:

: 93913-86-1
4-carboxy-N-(4'-pyridino) piperidine

: 1203600-34-3
4-[(benzyloxy)methyl]-1-(pyridin-4-yl)piperidine-4-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / 50 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

2.2: 2 h / 20 °C

3.1: water; sodium hydroxide / tetrahydrofuran; ethanol / 50 °C

With thionyl chloride; water; sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; ethanol;

Reference yield:

: 121912-29-6
1-(pyridin-4-yl)piperidine-4-carboxylic acid ethyl ester

: 1203600-34-3
4-[(benzyloxy)methyl]-1-(pyridin-4-yl)piperidine-4-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

1.2: 2 h / 20 °C

2.1: water; sodium hydroxide / tetrahydrofuran; ethanol / 50 °C

With water; sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; ethanol;