D-myo-Inositol, 1-O-(4-methoxyphenyl)methyl-2,6-bis-O-(phenylmethyl)-5-O-2-propenyl-3,4-O-(1S,2R,4S)-1,7,7-trimethylbicyclo2.2.1hept-2-ylidene-

Base Information

Chemical Name:D-myo-Inositol, 1-O-(4-methoxyphenyl)methyl-2,6-bis-O-(phenylmethyl)-5-O-2-propenyl-3,4-O-(1S,2R,4S)-1,7,7-trimethylbicyclo2.2.1hept-2-ylidene-
CAS No.:196302-93-9
Molecular Formula:C41H50O7
Molecular Weight:654.83
Hs Code.:
Mol file:196302-93-9.mol

Synonyms:D-myo-Inositol, 1-O-(4-methoxyphenyl)methyl-2,6-bis-O-(phenylmethyl)-5-O-2-propenyl-3,4-O-(1S,2R,4S)-1,7,7-trimethylbicyclo2.2.1hept-2-ylidene-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of D-myo-Inositol, 1-O-(4-methoxyphenyl)methyl-2,6-bis-O-(phenylmethyl)-5-O-2-propenyl-3,4-O-(1S,2R,4S)-1,7,7-trimethylbicyclo2.2.1hept-2-ylidene-

Chemical Property:

PSA：64.61000
LogP:7.66250

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Technology Process of D-myo-Inositol, 1-O-(4-methoxyphenyl)methyl-2,6-bis-O-(phenylmethyl)-5-O-2-propenyl-3,4-O-(1S,2R,4S)-1,7,7-trimethylbicyclo2.2.1hept-2-ylidene-

There total 10 articles about D-myo-Inositol, 1-O-(4-methoxyphenyl)methyl-2,6-bis-O-(phenylmethyl)-5-O-2-propenyl-3,4-O-(1S,2R,4S)-1,7,7-trimethylbicyclo2.2.1hept-2-ylidene- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 824-94-2
p-methoxybenzyl chloride

: 196302-92-8
1D-5-O-allyl-2,6-di-O-benzyl-3-O-endo,4-O-exo-(L-1',7',7'-trimethylbicyclo<2.2.1>hept-2'-ylidene)-myo-inositol

: 196302-93-9
1D-5-O-allyl-2,6-di-O-benzyl-1-O-(4'-methoxybenzyl)-3-O-endo,4-O-exo-(L-1',7',7'-trimethylbicyclo<2.2.1>hept-2'-ylidene)-myo-inositol

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; 1.) r.t., 20 min, 2.) r.t., 4 h;

Reference yield:

: 128525-51-9
(-)-camphor dimethyl acetal

: 196302-93-9
1D-5-O-allyl-2,6-di-O-benzyl-1-O-(4'-methoxybenzyl)-3-O-endo,4-O-exo-(L-1',7',7'-trimethylbicyclo<2.2.1>hept-2'-ylidene)-myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: 27 percent / p-TsOH*H₂O / CH₂Cl₂ / 1 h / Heating

2: 99 percent / NaH / dimethylformamide / 1.) r.t., 20 min, 2.) r.t., 4 h

With sodium hydride; toluene-4-sulfonic acid; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 100-39-0
benzyl bromide

: 196302-93-9
1D-5-O-allyl-2,6-di-O-benzyl-1-O-(4'-methoxybenzyl)-3-O-endo,4-O-exo-(L-1',7',7'-trimethylbicyclo<2.2.1>hept-2'-ylidene)-myo-inositol

Guidance literature:: Multi-step reaction with 6 steps

1: 93 percent / NaH / dimethylformamide / 1.) r.t., 1 h, 2.) r.t., 1 h

2: 94 percent / DIBAL-H / hexane; CH₂Cl₂ / 1.) 0 deg C, 15 min, 2.) r.t., 7 h

3: 94 percent / NaH, imidazole / dimethylformamide / 1.) r.t., 30 min, 2.) r.t., 24 h

4: 96 percent / HCl, H₂O / methanol / 2 h / Heating

5: 27 percent / p-TsOH*H₂O / CH₂Cl₂ / 1 h / Heating

6: 99 percent / NaH / dimethylformamide / 1.) r.t., 20 min, 2.) r.t., 4 h

With 1H-imidazole; hydrogenchloride; water; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; In methanol; hexane; dichloromethane; N,N-dimethyl-formamide;