3-bromo-5-(3-chloro-4-isopropoxyphenyl)-1,2,4-thiadiazole

Base Information

Chemical Name:3-bromo-5-(3-chloro-4-isopropoxyphenyl)-1,2,4-thiadiazole
CAS No.:1260023-56-0
Molecular Formula:C₁₁H₁₀BrClN₂OS
Molecular Weight:333.636
Hs Code.:
Mol file:1260023-56-0.mol

Synonyms:3-bromo-5-(3-chloro-4-isopropoxyphenyl)-1,2,4-thiadiazole

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Chemical Property of 3-bromo-5-(3-chloro-4-isopropoxyphenyl)-1,2,4-thiadiazole

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Technology Process of 3-bromo-5-(3-chloro-4-isopropoxyphenyl)-1,2,4-thiadiazole

There total 2 articles about 3-bromo-5-(3-chloro-4-isopropoxyphenyl)-1,2,4-thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 37159-60-7
3-bromo-5-chloro-[1,2,4]thiadiazole

: 1260023-79-7
2-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1260023-56-0
3-bromo-5-(3-chloro-4-isopropoxyphenyl)-1,2,4-thiadiazole

Guidance literature:: With potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In water; N,N-dimethyl-formamide; at 80 ℃; for 1h;
DOI:10.1021/jm2016107

Reference yield:

: 37159-60-7
3-bromo-5-chloro-[1,2,4]thiadiazole

: 480438-56-0
{3-chloro-4-[(1-methylethyl)oxy]phenyl}boronic acid

: 1260023-56-0
3-bromo-5-(3-chloro-4-isopropoxyphenyl)-1,2,4-thiadiazole

Guidance literature:: With potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In water; N,N-dimethyl-formamide; at 80 ℃; for 1h; Inert atmosphere; Sealed; Microwave irradiation;

Reference yield: 78.0%

: 1260023-56-0
3-bromo-5-(3-chloro-4-isopropoxyphenyl)-1,2,4-thiadiazole

: 1260023-43-5
2-ethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzaldehyde

: 1344997-59-6
3-(5-(3-chloro-4-isopropoxyphenyl)-1,2,4-thiadiazol-3-yl)-2-ethylbenzaldehyde

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; N,N-dimethyl-formamide; at 120 ℃; for 0.25h; Microwave irradiation;
DOI:10.1021/jm2016107