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37159-60-7 Usage

Chemical Properties

clear colorless to yellow liquid

Check Digit Verification of cas no

The CAS Registry Mumber 37159-60-7 includes 8 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 5 digits, 3,7,1,5 and 9 respectively; the second part has 2 digits, 6 and 0 respectively.
Calculate Digit Verification of CAS Registry Number 37159-60:
(7*3)+(6*7)+(5*1)+(4*5)+(3*9)+(2*6)+(1*0)=127
127 % 10 = 7
So 37159-60-7 is a valid CAS Registry Number.
InChI:InChI=1/C2BrClN2S/c3-1-5-2(4)7-6-1

37159-60-7SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 18, 2017

Revision Date: Aug 18, 2017

1.Identification

1.1 GHS Product identifier

Product name 3-Bromo-5-chloro-1,2,4-thiadiazole

1.2 Other means of identification

Product number -
Other names 3-BROMO-5-CHLORO-1,2,4-THIADIAZOLE

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:37159-60-7 SDS

37159-60-7Synthetic route

3,3'-dibromo-5,5'-disulfanediyl-bis-[1,2,4]thiadiazole
26542-78-9

3,3'-dibromo-5,5'-disulfanediyl-bis-[1,2,4]thiadiazole

3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

Conditions
ConditionsYield
With chlorine In acetic acid
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

N-(2,4-dimethoxybenzyl)-1-isopropyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazolo[4,3-c]pyridin-4-amine

N-(2,4-dimethoxybenzyl)-1-isopropyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazolo[4,3-c]pyridin-4-amine

3-(3-bromo-1,2,4-thiadiazol-5-yl)-N-(2.4-dimethoxybenzyl)-1-isopropyl-1H-pyrazolo[4,3-c]pyridin-4-amine

3-(3-bromo-1,2,4-thiadiazol-5-yl)-N-(2.4-dimethoxybenzyl)-1-isopropyl-1H-pyrazolo[4,3-c]pyridin-4-amine

Conditions
ConditionsYield
With potassium phosphate; tetrakis(triphenylphosphine) palladium(0) In 1,4-dioxane at 90℃; for 3h; Sealed tube;97%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

(4-benzyl-6-methyl-pyrimidin-2-yl)-piperidin-4-yl-amine hydrochloride

(4-benzyl-6-methyl-pyrimidin-2-yl)-piperidin-4-yl-amine hydrochloride

(4-Benzyl-6-methyl-pyrimidin-2-yl)-[1-(3-bromo-[1,2,4]thiadiazol-5-yl)-piperidin-4-yl]-amine
1329669-67-1

(4-Benzyl-6-methyl-pyrimidin-2-yl)-[1-(3-bromo-[1,2,4]thiadiazol-5-yl)-piperidin-4-yl]-amine

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 95℃; for 4.5h;96%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

(4-benzyl-6-methyl-pyrimidin-2-yl)-piperidin-4-yl-amine hydrochloride
1329673-47-3

(4-benzyl-6-methyl-pyrimidin-2-yl)-piperidin-4-yl-amine hydrochloride

(4-Benzyl-6-methyl-pyrimidin-2-yl)-[1-(3-bromo-[1,2,4]thiadiazol-5-yl)-piperidin-4-yl]-amine
1329669-67-1

(4-Benzyl-6-methyl-pyrimidin-2-yl)-[1-(3-bromo-[1,2,4]thiadiazol-5-yl)-piperidin-4-yl]-amine

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 95℃; for 4.5h;96%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2-(trifluoromethyl)phenyl)piperidine
1373522-74-7

1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2-(trifluoromethyl)phenyl)piperidine

3-bromo-5-(4-(piperidin-1-yl)-3-(trifluoromethyl)phenyl)-1,2,4-thiadiazole
1373522-75-8

3-bromo-5-(4-(piperidin-1-yl)-3-(trifluoromethyl)phenyl)-1,2,4-thiadiazole

Conditions
ConditionsYield
With potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 In water; N,N-dimethyl-formamide at 80℃; for 1h; Suzuki coupling;94%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

4-(3-(phenylsulfonyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)morpholine

4-(3-(phenylsulfonyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)morpholine

4-(3-(3-bromo-1,2,4-thiadiazol-5-yl)-5-(phenylsulfonyl)phenyl)morpholine

4-(3-(3-bromo-1,2,4-thiadiazol-5-yl)-5-(phenylsulfonyl)phenyl)morpholine

Conditions
ConditionsYield
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; cesium fluoride In 1,4-dioxane; water at 80℃;91%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

(2-(9H-carbazol-9-yl)phenyl)boronic acid
1189047-28-6

(2-(9H-carbazol-9-yl)phenyl)boronic acid

3,5-bis(2-(9H-carbazol-9-yl)phenyl)-1,2,4-thiadiazole
1567346-70-6

3,5-bis(2-(9H-carbazol-9-yl)phenyl)-1,2,4-thiadiazole

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; toluene at 100℃; for 24h; Suzuki Coupling;89%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran for 12h; Inert atmosphere; Sonication;89%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

2-(2-methylpropyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzonitrile
856167-68-5

2-(2-methylpropyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzonitrile

5-(3-bromo-1,2,4-thiadiazol-5-yl)-2-isobutylbenzonitrile
1344997-62-1

5-(3-bromo-1,2,4-thiadiazol-5-yl)-2-isobutylbenzonitrile

Conditions
ConditionsYield
With potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 In water; N,N-dimethyl-formamide at 80℃; for 1h; Suzuki coupling;88%
With potassium phosphate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In water; N,N-dimethyl-formamide at 80℃; for 1h; Suzuki Coupling; Inert atmosphere; Microwave irradiation; Sealed vessel;
With potassium phosphate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In water; N,N-dimethyl-formamide at 80℃; for 1h; Inert atmosphere; Sealed; microwave irradiation;
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

1-phenyl-2-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1H-benzo[d]imidazole
952514-86-2

1-phenyl-2-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1H-benzo[d]imidazole

3,5-bis(3-(1-phenyl-1H-benzo[d]imidazol-2-yl)phenyl)-1,2,4-thiadiazole

3,5-bis(3-(1-phenyl-1H-benzo[d]imidazol-2-yl)phenyl)-1,2,4-thiadiazole

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 100℃; for 12h; Suzuki Coupling; Inert atmosphere;88%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

4,4,5,5-tetramethyl-2-(2-(trifluoromethyl)-[1,1'-biphenyl]-4-yl)-1,3,2-dioxaborolane
1373522-76-9

4,4,5,5-tetramethyl-2-(2-(trifluoromethyl)-[1,1'-biphenyl]-4-yl)-1,3,2-dioxaborolane

3-bromo-5-(2-(trifluoromethyl)-[1,1'-biphenyl]-4-yl)-1,2,4-thiadiazole
1373522-77-0

3-bromo-5-(2-(trifluoromethyl)-[1,1'-biphenyl]-4-yl)-1,2,4-thiadiazole

Conditions
ConditionsYield
With potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 In water; N,N-dimethyl-formamide at 80℃; for 1h; Suzuki coupling;86%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

1-(4-methoxyphenethyl)piperazine dihydrochloride

1-(4-methoxyphenethyl)piperazine dihydrochloride

1-(3-bromo-[1,2,4]thiadiazol-5-yl)-4-[2-(4-methoxy-phenyl)-ethyl]-piperazine
1417825-20-7

1-(3-bromo-[1,2,4]thiadiazol-5-yl)-4-[2-(4-methoxy-phenyl)-ethyl]-piperazine

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In ethanol at 20℃;85%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

(5,10-diphenyl-5,10-dihydrophenazine-2-yl)boronic acid

(5,10-diphenyl-5,10-dihydrophenazine-2-yl)boronic acid

C50H34N6S

C50H34N6S

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 85℃; for 28h; Inert atmosphere;85%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

(3-(9,9-dimethylacridin-10(9H)-yl)phenyl)boronic acid

(3-(9,9-dimethylacridin-10(9H)-yl)phenyl)boronic acid

C44H36N4S

C44H36N4S

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 50 - 100℃; Inert atmosphere;85%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 50 - 100℃; Inert atmosphere;85%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

phenanthrene-3-ylboronic acid
1188094-46-3

phenanthrene-3-ylboronic acid

C30H18N2S

C30H18N2S

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 85℃; for 28h; Inert atmosphere;85%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

phenylboronic acid
98-80-6

phenylboronic acid

3-bromo-5-phenyl-1,2,4-thiadiazole
101495-43-6

3-bromo-5-phenyl-1,2,4-thiadiazole

Conditions
ConditionsYield
With bis(di-tert-butyl(4-dimethylaminophenyl)phosphine)dichloropalladium(II); cesium fluoride In 1,4-dioxane; water at 80℃; for 16h; Inert atmosphere;84%
With bis(di-tert-butyl(4-dimethylaminophenyl)phosphine)dichloropalladium(II); cesium fluoride In 1,4-dioxane; water at 80℃; for 16h; Suzuki-Miyaura coupling; Inert atmosphere;71%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

3-(9H-carbazol-9-yl)phenylboronic acid
864377-33-3

3-(9H-carbazol-9-yl)phenylboronic acid

3,5-bis(3-(9H-carbazol-9-yl)phenyl)-1,2,4-thiadiazole
1567346-71-7

3,5-bis(3-(9H-carbazol-9-yl)phenyl)-1,2,4-thiadiazole

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; toluene at 100℃; for 24h; Suzuki Coupling;84%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran for 12h; Inert atmosphere; Sonication;84%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

C22H22BNO2S

C22H22BNO2S

C46H40N4S3

C46H40N4S3

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 85℃; for 28h; Inert atmosphere;84%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

(9-(dibenzo[b,d]thiophen-3-yl)-9H-carbazol-3-yl)boronic acid

(9-(dibenzo[b,d]thiophen-3-yl)-9H-carbazol-3-yl)boronic acid

C50H28N4S3

C50H28N4S3

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 85℃; for 28h; Inert atmosphere;82%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

C25H22BNO2

C25H22BNO2

C52H40N4S

C52H40N4S

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 85℃; for 28h; Inert atmosphere;81%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

(4-(3-phenyl-9H-carbazol-9-yl)phenyl)boronic acid

(4-(3-phenyl-9H-carbazol-9-yl)phenyl)boronic acid

C50H32N4S

C50H32N4S

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; (2)H8-toluene; water at 50 - 100℃; Inert atmosphere;81%
4-(carbazol-9-yl)phenylboronic acid
419536-33-7

4-(carbazol-9-yl)phenylboronic acid

3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

3,5-bis(4-(9H-carbazol-9-yl)phenyl)-1,2,4-thiadiazole
1567346-72-8

3,5-bis(4-(9H-carbazol-9-yl)phenyl)-1,2,4-thiadiazole

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; toluene at 100℃; for 24h; Suzuki Coupling;80%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

(3-(dibenzothiophen-2-yl(phenyl)amine)phenyl)boronic acid

(3-(dibenzothiophen-2-yl(phenyl)amine)phenyl)boronic acid

C50H32N4S3

C50H32N4S3

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 50 - 100℃; Inert atmosphere;80%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 50 - 100℃; Inert atmosphere;80%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

4-tert-butylphenylboronic acid
123324-71-0

4-tert-butylphenylboronic acid

3-bromo-5-(4-(tert-butyl)phenyl)-1,2,4-thiadiazole

3-bromo-5-(4-(tert-butyl)phenyl)-1,2,4-thiadiazole

Conditions
ConditionsYield
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate In toluene at 100℃; for 12h; Reflux; Inert atmosphere;78%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

(E)-4-(2-(3-azabicyclo[3.1.0]hexan-6-yl)vinyl)-5-cyclopropyl-3-(3,5-dichloropyridin-4-yl)isoxazole

(E)-4-(2-(3-azabicyclo[3.1.0]hexan-6-yl)vinyl)-5-cyclopropyl-3-(3,5-dichloropyridin-4-yl)isoxazole

(E)-4-(2-(3-(3-bromo-1,2,4-thiadiazol-5-yl)-3-azabicyclo[3.1.0]hexan-6-yl)vinyl)-5-cyclopropyl-3-(3,5-dichloropyridin-4-yl)isoxazole

(E)-4-(2-(3-(3-bromo-1,2,4-thiadiazol-5-yl)-3-azabicyclo[3.1.0]hexan-6-yl)vinyl)-5-cyclopropyl-3-(3,5-dichloropyridin-4-yl)isoxazole

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 20℃; for 2h;78%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

(4-(3-(naphthalen-2-yl)-9H-carbazol-9-yl)phenyl)boronic acid

(4-(3-(naphthalen-2-yl)-9H-carbazol-9-yl)phenyl)boronic acid

3-bromo-5-(4-(3-(naphthalen-2-yl)-9H-carbazol-9-yl)phenyl)-1,2,4-thiadiazole

3-bromo-5-(4-(3-(naphthalen-2-yl)-9H-carbazol-9-yl)phenyl)-1,2,4-thiadiazole

Conditions
ConditionsYield
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate In toluene at 90℃; for 24h; Inert atmosphere;77%
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate In toluene at 90℃; for 24h; Inert atmosphere;77%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

3,4-Dimethoxyphenylboronic acid
122775-35-3

3,4-Dimethoxyphenylboronic acid

3-bromo-5-(3,4-dimethoxyphenyl)-1,2,4-thiadiazole

3-bromo-5-(3,4-dimethoxyphenyl)-1,2,4-thiadiazole

Conditions
ConditionsYield
With potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 In water; N,N-dimethyl-formamide at 80℃; for 2h; Microwave irradiation;77%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

(4-thiomethoxyphenyl)boronic acid
98546-51-1

(4-thiomethoxyphenyl)boronic acid

C9H7BrN2S2
1198321-26-4

C9H7BrN2S2

Conditions
ConditionsYield
With bis(di-tert-butyl(4-dimethylaminophenyl)phosphine)dichloropalladium(II); cesium fluoride In 1,4-dioxane; water at 80℃; for 16h; Suzuki-Miyaura coupling; Inert atmosphere;72%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

4-(diphenylamino)phenyl boronic acid
201802-67-7

4-(diphenylamino)phenyl boronic acid

4-(3-bromo-1,2,4-thiadiazol-5-yl)-N,N-diphenylaniline

4-(3-bromo-1,2,4-thiadiazol-5-yl)-N,N-diphenylaniline

Conditions
ConditionsYield
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate In toluene at 50 - 100℃; Inert atmosphere;72%
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate In toluene at 50 - 100℃; Inert atmosphere;72%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

(2-(9H-carbazol-9-yl)phenyl)boronic acid
1189047-28-6

(2-(9H-carbazol-9-yl)phenyl)boronic acid

5-(2-(9H-carbazol-9-yl)phenyl)-3-bromo-1,2,4-thiadiazole

5-(2-(9H-carbazol-9-yl)phenyl)-3-bromo-1,2,4-thiadiazole

Conditions
ConditionsYield
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate In toluene at 100℃; for 12h; Inert atmosphere;71%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

2-(3-{3-[5-benzyloxy-2-ethyl-4-(4,4,5,5-tetramethyl-[1,3,2]diaxabarolan-2-yl)phenoxy]propoxy}-2-propylphenoxy)benzoic acid methyl ester
339529-96-3

2-(3-{3-[5-benzyloxy-2-ethyl-4-(4,4,5,5-tetramethyl-[1,3,2]diaxabarolan-2-yl)phenoxy]propoxy}-2-propylphenoxy)benzoic acid methyl ester

2-(3-{3-[5-benzyloxy-4-(3-bromo-[1,2,4]thiadiazol-5-yl)-2-ethyl-phenoxy]propoxy}-2-propylphenoxy)benzoic acid methyl ester
339529-97-4

2-(3-{3-[5-benzyloxy-4-(3-bromo-[1,2,4]thiadiazol-5-yl)-2-ethyl-phenoxy]propoxy}-2-propylphenoxy)benzoic acid methyl ester

Conditions
ConditionsYield
With caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In toluene at 100℃; for 15h;70%
3-bromo-5-chloro-[1,2,4]thiadiazole
37159-60-7

3-bromo-5-chloro-[1,2,4]thiadiazole

4-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2-(trifluoromethyl)phenyl)morpholine
1373522-71-4

4-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2-(trifluoromethyl)phenyl)morpholine

4-(4-(3-bromo-1,2,4-thiadiazol-5-yl)-2-(trifluoromethyl)phenyl)morpholine
1373522-72-5

4-(4-(3-bromo-1,2,4-thiadiazol-5-yl)-2-(trifluoromethyl)phenyl)morpholine

Conditions
ConditionsYield
With potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 In water; N,N-dimethyl-formamide at 80℃; for 1h; Suzuki coupling;69%

37159-60-7Relevant articles and documents

Certain 3,5-dihalo-1,2,4-thiadiazole preparations

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, (2008/06/13)

3,5-Dihalo-1,2,4-thiadiazoles and their preparation from corresponding 5 alkylthio compounds, useful as intermediates for fumigants are disclosed.

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