5,5'-Methylenediisophthalic acid

Base Information

Chemical Name:5,5'-Methylenediisophthalic acid
CAS No.:10397-52-1
Molecular Formula:C17H12O8
Molecular Weight:344.277
Hs Code.:2917399090
European Community (EC) Number:664-393-6
DSSTox Substance ID:DTXSID50578789
Nikkaji Number:J2.651.493B
Wikidata:Q82469111
Mol file:10397-52-1.mol

Synonyms:10397-52-1;5,5'-Methylenediisophthalic acid;5-[(3,5-DICARBOXYPHENYL)METHYL]BENZENE-1,3-DICARBOXYLIC ACID;MFCD19053170;1,3-Benzenedicarboxylic acid, 5,5'-methylenebis-;Linker for PCN-12 MOF;3,3',5,5'-tetracarboxydiphenylmethane;YSZC711;SCHEMBL1950244;DTXSID50578789;5,5'-methylene diisophthalic acid;AC9718;AKOS034832937;5,5?-METHYLENEDIISOPHTHALIC ACID;BS-46515;SY261902;5,5'-Methylenediisophthalic acid - H4MDIP;CS-0169944;5,5'-Methylenedi(benzene-1,3-dicarboxylic acid);3,3',5,5'-Tetracarboxydiphenylmethane, >=95% (HPLC);5,5 inverted exclamation mark -Methylenediisophthalic Acid

Suppliers and Price of 5,5'-Methylenediisophthalic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
3,3′,5,5′-Tetracarboxydiphenylmethane ≥95% (HPLC)
500mg
$ 127.00

Ambeed
5,5'-Methylenediisophthalicacid 98%
5g
$ 982.00

Ambeed
5,5'-Methylenediisophthalicacid 98%
1g
$ 234.00

Ambeed
5,5'-Methylenediisophthalicacid 98%
250mg
$ 95.00

Ambeed
5,5'-Methylenediisophthalicacid 98%
100mg
$ 68.00

Total 12 raw suppliers

Chemical Property of 5,5'-Methylenediisophthalic acid

Chemical Property:

Melting Point:324-331°C
Boiling Point:729.5±60.0 °C(Predicted)
PSA：149.20000
Density:1.572±0.06 g/cm3(Predicted)
LogP:2.07020
XLogP3:1.9
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:6
Exact Mass:344.05321734
Heavy Atom Count:25
Complexity:465

Purity/Quality:

98%,99%, ^*data from raw suppliers

3,3′,5,5′-Tetracarboxydiphenylmethane ≥95% (HPLC) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C=C(C=C1C(=O)O)C(=O)O)CC2=CC(=CC(=C2)C(=O)O)C(=O)O

Technology Process of 5,5'-Methylenediisophthalic acid

There total 4 articles about 5,5'-Methylenediisophthalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 10397-51-0
3,3',5,5'-tetrakis(methoxycarbonyl)diphenylmethane

: 10397-52-1
3,3’,5,5’-tetracarboxydiphenylmethane

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; for 1h; Heating;
DOI:10.1002/ejoc.200700295

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 121-91-5
isophthalic acid

: 10397-52-1
3,3’,5,5’-tetracarboxydiphenylmethane

Guidance literature:: With sulfuric acid; sulfur trioxide; at 0 - 118 ℃; for 6h; Product distribution / selectivity;

Reference yield:

: 121-91-5
isophthalic acid

: 10397-52-1
3,3’,5,5’-tetracarboxydiphenylmethane

Guidance literature:: Multi-step reaction with 2 steps

1: 12 percent / oleum / 6 h / 118 °C

2: 91 percent / NaOH / tetrahydrofuran; H₂O / 1 h / Heating

With sodium hydroxide; sulfuric acid; In tetrahydrofuran; water;
DOI:10.1002/ejoc.200700295