CH3SO3H

Base Information

Chemical Name:CH3SO3H
CAS No.:1236208-20-0
Molecular Formula:2CH₄O₃S*C₁₆H₁₉N₃S
Molecular Weight:477.627
Hs Code.:
Mol file:1236208-20-0.mol

Synonyms:Leucomethylene blue (Mesylate);N3,N3,N7,N7-Tetramethyl-10H-phenothiazine-3,7-diamine methanesulfonate (1:2);TRx0237 (LMTX) mesylate

Suppliers and Price of CH3SO3H

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

DC Chemicals
TRx0237(LMTX)mesylate >98%
1 g
$ 1000.00

DC Chemicals
TRx0237(LMTX)mesylate >98%
100 mg
$ 250.00

CSNpharm
LeucomethyleneBlueMesylate
5mg
$ 48.00

Crysdot
LeucomethyleneBlueMesylate 97%
5mg
$ 40.00

Crysdot
LeucomethyleneBlueMesylate 97%
50mg
$ 173.00

Crysdot
LeucomethyleneBlueMesylate 97%
10mg
$ 55.00

Total 16 raw suppliers

Chemical Property of CH3SO3H

Chemical Property:

PSA：169.31000
LogP:5.33440

Purity/Quality:

99%, ^*data from raw suppliers

TRx0237(LMTX)mesylate >98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of CH3SO3H

There total 3 articles about CH3SO3H which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 75-75-2,98527-29-8
methanesulfonic acid

: 3763-06-2
1-[3,7-bis(dimethylamino)phenothiazin-10-yl]ethanone

: 1236208-20-0
leucomethylthioninium bis(hydromethanesulfonate)

Guidance literature:: 1-[3,7-bis(dimethylamino)phenothiazin-10-yl]ethanone; In toluene; for 0.5h; Reflux;

methanesulfonic acid; In water; toluene; at 85 ℃; for 3h; Product distribution / selectivity;

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 75-75-2,98527-29-8
methanesulfonic acid

: 1747-90-6
3,11-dinitro-10H-phenothiazine

: 1236208-20-0
leucomethylthioninium bis(hydromethanesulfonate)

Guidance literature:: 3,11-dinitro-10H-phenothiazine; With 5%-palladium/activated carbon; hydrogen; In water; N,N-dimethyl-formamide; at 20 ℃; for 1.5h; under 2775.28 - 15301.5 Torr;

formaldehyd; With hydrogen; In water; N,N-dimethyl-formamide; at 90 ℃; for 24h; under 2700.27 Torr;

methanesulfonic acid; In methanol; ethanol; toluene; at 5 ℃; for 2h; Inert atmosphere;

Reference yield:

: 152071-32-4,105504-42-5,121067-62-7,12262-49-6,167498-52-4,6476-03-5,97130-83-1
methylene blue

: 1236208-20-0
leucomethylthioninium bis(hydromethanesulfonate)

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; hydrazine hydrate / acetonitrile / 2 h / 15 - 70 °C / Industry scale

1.2: 2 h / 90 - 100 °C / Industry scale

2.1: toluene / 0.5 h / Reflux

2.2: 3 h / 85 °C

With hydrazine hydrate; triethylamine; In toluene; acetonitrile;