1-[4-(Benzenesulfonyl)-3-methylbut-2-en-1-yl]-2,3,4,5-tetramethoxy-6-methylbenzene

Base Information

Chemical Name:1-[4-(Benzenesulfonyl)-3-methylbut-2-en-1-yl]-2,3,4,5-tetramethoxy-6-methylbenzene
CAS No.:73875-21-5
Molecular Formula:C21H26O5S
Molecular Weight:420.527
Hs Code.:
DSSTox Substance ID:DTXSID10699707
Mol file:73875-21-5.mol

Synonyms:73875-21-5;DTXSID10699707;1-[4-(Benzenesulfonyl)-3-methylbut-2-en-1-yl]-2,3,4,5-tetramethoxy-6-methylbenzene

Suppliers and Price of 1-[4-(Benzenesulfonyl)-3-methylbut-2-en-1-yl]-2,3,4,5-tetramethoxy-6-methylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[4-(Benzenesulfonyl)-3-methylbut-2-en-1-yl]-2,3,4,5-tetramethoxy-6-methylbenzene

Chemical Property:

PSA：79.44000
LogP:5.07290
XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:9
Exact Mass:420.16065978
Heavy Atom Count:29
Complexity:620

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=C(C(=C1OC)OC)OC)OC)CC=C(C)CS(=O)(=O)C2=CC=CC=C2

Technology Process of 1-[4-(Benzenesulfonyl)-3-methylbut-2-en-1-yl]-2,3,4,5-tetramethoxy-6-methylbenzene

There total 7 articles about 1-[4-(Benzenesulfonyl)-3-methylbut-2-en-1-yl]-2,3,4,5-tetramethoxy-6-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59277-17-7
1-(benzenesulfonyl)-2-methyl-4-chloro-2-butene

: 35896-58-3
2,3,4,5-tetramethoxytoluene

: 73875-21-5
(2'E)-1-(3'-methyl-4'-phenylsulfonylbut-2'-enyl)-6-methyl-2,3,4,5-tetramethoxybenzene

: (2'Z)-1-(3'-methyl-4'-phenylsulfonylbut-2'-enyl)-6-methyl-2,3,4,5-tetramethoxybenzene

Guidance literature:: With montmollironite K-10; In water; 1,2-dichloro-ethane; at 85 ℃; for 18h; Reagent/catalyst; Temperature; Time; Solvent; stereoselective reaction; Large scale;
DOI:10.5012/bkcs.2013.34.4.1257

Reference yield:

: 59277-17-7
1-(benzenesulfonyl)-2-methyl-4-chloro-2-butene

: 35896-58-3
2,3,4,5-tetramethoxytoluene

: 73875-21-5
(2'E)-1-(3'-methyl-4'-phenylsulfonylbut-2'-enyl)-6-methyl-2,3,4,5-tetramethoxybenzene

Guidance literature:: With montmollironite K-10; In neat (no solvent); at 80 ℃; for 16h; Time; stereoselective reaction;
DOI:10.5012/bkcs.2013.34.4.1257

Reference yield:

: 78-79-5,9003-31-0
isoprene

: 73875-21-5
(2'E)-1-(3'-methyl-4'-phenylsulfonylbut-2'-enyl)-6-methyl-2,3,4,5-tetramethoxybenzene

: (2'Z)-1-(3'-methyl-4'-phenylsulfonylbut-2'-enyl)-6-methyl-2,3,4,5-tetramethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine hydrochloride; copper dichloride / acetonitrile / 8 h / 80 °C

2: iron(III) chloride / dichloromethane / 8 h / 40 °C

With iron(III) chloride; triethylamine hydrochloride; copper dichloride; In dichloromethane; acetonitrile; 2: |Friedel-Crafts Alkylation;
DOI:10.1002/ejoc.201200627