(2'E,6'E,10'E,14'E,18'E,22'E,26'E,30'E,34'E,38'E)-1-(3,7',11',15',19',23',27',31',35',39'-decamethyl-4'-phenylsulfonyltetraconta-2',6',10',14',18',22',26',30',34',38'-decaenyl)-6-methyl-2,3,4,5-tetramethoxybenzene

Base Information

Chemical Name:(2'E,6'E,10'E,14'E,18'E,22'E,26'E,30'E,34'E,38'E)-1-(3,7',11',15',19',23',27',31',35',39'-decamethyl-4'-phenylsulfonyltetraconta-2',6',10',14',18',22',26',30',34',38'-decaenyl)-6-methyl-2,3,4,5-tetramethoxybenzene
CAS No.:618457-07-1
Molecular Formula:C₆₇H₁₀₀O₆S
Molecular Weight:1033.59
Hs Code.:

(2'E,6'E,10'E,14'E,18'E,22'E,26'E,30'E,34'E,38'E)-1-(3,7',11',15',19',23',27',31',35',39'-decamethyl-4'-phenylsulfonyltetraconta-2',6',10',14',18',22',26',30',34',38'-decaenyl)-6-methyl-2,3,4,5-tetramethoxybenzene

Synonyms:(2'E,6'E,10'E,14'E,18'E,22'E,26'E,30'E,34'E,38'E)-1-(3,7',11',15',19',23',27',31',35',39'-decamethyl-4'-phenylsulfonyltetraconta-2',6',10',14',18',22',26',30',34',38'-decaenyl)-6-methyl-2,3,4,5-tetramethoxybenzene

Suppliers and Price of (2'E,6'E,10'E,14'E,18'E,22'E,26'E,30'E,34'E,38'E)-1-(3,7',11',15',19',23',27',31',35',39'-decamethyl-4'-phenylsulfonyltetraconta-2',6',10',14',18',22',26',30',34',38'-decaenyl)-6-methyl-2,3,4,5-tetramethoxybenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2'E,6'E,10'E,14'E,18'E,22'E,26'E,30'E,34'E,38'E)-1-(3,7',11',15',19',23',27',31',35',39'-decamethyl-4'-phenylsulfonyltetraconta-2',6',10',14',18',22',26',30',34',38'-decaenyl)-6-methyl-2,3,4,5-tetramethoxybenzene

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Technology Process of (2'E,6'E,10'E,14'E,18'E,22'E,26'E,30'E,34'E,38'E)-1-(3,7',11',15',19',23',27',31',35',39'-decamethyl-4'-phenylsulfonyltetraconta-2',6',10',14',18',22',26',30',34',38'-decaenyl)-6-methyl-2,3,4,5-tetramethoxybenzene

There total 2 articles about (2'E,6'E,10'E,14'E,18'E,22'E,26'E,30'E,34'E,38'E)-1-(3,7',11',15',19',23',27',31',35',39'-decamethyl-4'-phenylsulfonyltetraconta-2',6',10',14',18',22',26',30',34',38'-decaenyl)-6-methyl-2,3,4,5-tetramethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 52610-77-2
solanesyl bromide

: 73875-21-5
(2'E)-1-(3'-methyl-4'-phenylsulfonylbut-2'-enyl)-6-methyl-2,3,4,5-tetramethoxybenzene

: 618457-07-1
(2'E,6'E,10'E,14'E,18'E,22'E,26'E,30'E,34'E,38'E)-1-(3,7',11',15',19',23',27',31',35',39'-decamethyl-4'-phenylsulfonyltetraconta-2',6',10',14',18',22',26',30',34',38'-decaenyl)-6-methyl-2,3,4,5-tetramethoxybenzene

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;
DOI:10.1021/jo0350155

Reference yield:

: 13190-97-1,540-03-4
solanesol

: 618457-07-1
(2'E,6'E,10'E,14'E,18'E,22'E,26'E,30'E,34'E,38'E)-1-(3,7',11',15',19',23',27',31',35',39'-decamethyl-4'-phenylsulfonyltetraconta-2',6',10',14',18',22',26',30',34',38'-decaenyl)-6-methyl-2,3,4,5-tetramethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: PBr₃

2: 90 percent / n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

With n-butyllithium; phosphorus tribromide; In tetrahydrofuran; hexane;
DOI:10.1021/jo0350155

Reference yield: 77.0%

: 618457-07-1
(2'E,6'E,10'E,14'E,18'E,22'E,26'E,30'E,34'E,38'E)-1-(3,7',11',15',19',23',27',31',35',39'-decamethyl-4'-phenylsulfonyltetraconta-2',6',10',14',18',22',26',30',34',38'-decaenyl)-6-methyl-2,3,4,5-tetramethoxybenzene

: 94828-17-8
(2'E,6'E,10'E,14'E,18'E,22'E,26'E,30'E,34'E,38'E)-1-(3',7',11',15',19',23',27',31',35',39'-decamethyltetraconta-2',6',10',14',18',22',26',30',34',38'-decaenyl)-6-methyl-2,3,4,5-tetramethoxybenzene

Guidance literature:: With (1,2-bis(diphenylphosphanyl)ethane)dichloridopalladium(II); lithium triethylborohydride; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/jo0350155