TRANS-2-NONENAL 2,4-DINITROPHENYLHYDRAZONE

Base Information

• Chemical Name: TRANS-2-NONENAL 2,4-DINITROPHENYLHYDRAZONE
• CAS No.: 18287-00-8
• Molecular Formula: C₁₅H₂₀N₄O₄
• Molecular Weight: 320.348
• Mol file: 18287-00-8.mol

Synonyms:TRANS-2-NONENAL 2,4-DINITROPHENYLHYDRAZONE

Chemical Property of TRANS-2-NONENAL 2,4-DINITROPHENYLHYDRAZONE

Chemical Property:

• Melting Point: 124 - 125 °C
• PSA: 116.03000
• LogP: 5.54670

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of TRANS-2-NONENAL 2,4-DINITROPHENYLHYDRAZONE

There total 4 articles about TRANS-2-NONENAL 2,4-DINITROPHENYLHYDRAZONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2,4-dinitro-phenyl)-hydrazine (119-26-6) → non-2t-enal-(2,4-dinitro-phenylhydrazone) (18287-00-8)

Guidance literature:

With sulfuric acid;

DOI:10.1007/BF01167149 DOI:10.1021/ja01561a028

Reference yield:

heptanal (111-71-7) → non-2t-enal-(2,4-dinitro-phenylhydrazone) (18287-00-8)

Guidance literature:

Multi-step reaction with 2 steps

1: boron fluoride; diethyl ether / und anschliessenden Erhitzen mit wss.Schwefelsaeure

With diethyl ether; boron trifluoride;

DOI:10.1002/hlca.19560390517

Reference yield:

n-hexylmagnesium bromide (3761-92-0) → non-2t-enal-(2,4-dinitro-phenylhydrazone) (18287-00-8)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether; benzene

With diethyl ether; benzene;

upstream raw materials:

(E)-2-Nonenal

(2,4-dinitro-phenyl)-hydrazine

n-hexylmagnesium bromide

heptanal