N-(Diphenylphosphinyl-α-(p-tosyl)benzyl amine

Base Information

Chemical Name:N-(Diphenylphosphinyl-α-(p-tosyl)benzyl amine
CAS No.:701291-86-3
Molecular Formula:C26H24NO3PS
Molecular Weight:461.51
Hs Code.:
Mol file:701291-86-3.mol

Synonyms:N-(Diphenylphosphinyl-α-(p-tosyl)benzyl amine;N-[α-(4-Methylphenyl)sulfonyl)benzyl]diphenylphosphinic amide

Suppliers and Price of N-(Diphenylphosphinyl-α-(p-tosyl)benzyl amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
N-[α-(4-Methylphenyl)sulfonyl)benzyl]diphenylphosphinic amide
100mg
$ 55.00

Sigma-Aldrich
N-[α-(4-Methylphenyl)sulfonyl)benzyl]diphenylphosphinic amide 95%
1g
$ 75.40

AK Scientific
N-[α-(4-Methylphenyl)sulfonyl)benzyl]diphenylphosphinic amide
1g
$ 149.00

Total 2 raw suppliers

Chemical Property of N-(Diphenylphosphinyl-α-(p-tosyl)benzyl amine

Chemical Property:

Melting Point:140-144 °C
Boiling Point:656.4±65.0 °C(Predicted)
PKA:-3.13±0.70(Predicted)
PSA：81.43000
Density:1.30±0.1 g/cm3(Predicted)
LogP:6.45790

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

N-[α-(4-Methylphenyl)sulfonyl)benzyl]diphenylphosphinic amide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xn
Statements: 22

MSDS Files:: SDS file from LookChem

Useful:

Uses N-[α-(4-Methylphenyl)sulfonyl)benzyl]diphenylphosphinic Amide is a useful reagent for the synthesis of organic intermediates.

Technology Process of N-(Diphenylphosphinyl-α-(p-tosyl)benzyl amine

There total 2 articles about N-(Diphenylphosphinyl-α-(p-tosyl)benzyl amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 536-57-2
p-toluene sulfinic acid

: 5994-87-6
diphenylphosphinamide

: 100-52-7
benzaldehyde

: 701291-86-3
N-[(4-methylphenyl)sulfonyl](phenyl)methyl-P,P-diphenylphosphinic amide

Guidance literature:: In diethyl ether; dichloromethane; at 20 ℃; for 48h;
DOI:10.15227/orgsyn.083.0005

Reference yield: 90.0%

: 536-57-2
p-toluene sulfinic acid

: 98837-46-8,67764-52-7
P,P-diphenyl-N-(phenylmethylene)phosphinic amide

: 701291-86-3
N-[(4-methylphenyl)sulfonyl](phenyl)methyl-P,P-diphenylphosphinic amide

Guidance literature:: In diethyl ether; dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/ol5024807

Reference yield: 82.0%

: 701291-86-3
N-[(4-methylphenyl)sulfonyl](phenyl)methyl-P,P-diphenylphosphinic amide

: 1122-91-4
4-bromo-benzaldehyde

: N-(2-(4-bromophenyl)-2-oxo-1-phenylethyl)-P,P-diphenylphosphinic amide

Guidance literature:: With bis(diethylamino)cyclopropenium tetraphenylborate; caesium carbonate; In acetonitrile; at 20 ℃; for 16h; Schlenk technique; Molecular sieve; Inert atmosphere;
DOI:10.1021/ol5024807