(3aS)-5β-[(4R)-2,2-Dimethyl-1,3-dioxolan-4-yl]-3aβ,5,6,6aβ-tetrahydro-2-phenylfuro[3,2-d]oxazol-6β-ol

Base Information

Chemical Name:(3aS)-5β-[(4R)-2,2-Dimethyl-1,3-dioxolan-4-yl]-3aβ,5,6,6aβ-tetrahydro-2-phenylfuro[3,2-d]oxazol-6β-ol
CAS No.:23661-45-2
Molecular Formula:C₁₆H₁₉NO₅
Molecular Weight:305.33
Hs Code.:
Mol file:23661-45-2.mol

Synonyms:(3aS)-5β-[(4R)-2,2-Dimethyl-1,3-dioxolan-4-yl]-3aβ,5,6,6aβ-tetrahydro-2-phenylfuro[3,2-d]oxazol-6β-ol

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Chemical Property of (3aS)-5β-[(4R)-2,2-Dimethyl-1,3-dioxolan-4-yl]-3aβ,5,6,6aβ-tetrahydro-2-phenylfuro[3,2-d]oxazol-6β-ol

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Technology Process of (3aS)-5β-[(4R)-2,2-Dimethyl-1,3-dioxolan-4-yl]-3aβ,5,6,6aβ-tetrahydro-2-phenylfuro[3,2-d]oxazol-6β-ol

There total 11 articles about (3aS)-5β-[(4R)-2,2-Dimethyl-1,3-dioxolan-4-yl]-3aβ,5,6,6aβ-tetrahydro-2-phenylfuro[3,2-d]oxazol-6β-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 6847-14-9,14086-91-0,19949-63-4,61949-16-4
N-benzoyl-D-glucosamine

: 67-64-1
acetone

: 23661-45-2
2-phenyl-4,5-(5,6-isopropylidene-D-glucofurano)-1,3-oxazoline

Guidance literature:: With iron(III) chloride;
DOI:10.1016/S0014-827X(03)00022-3

Reference yield:

: 1078691-95-8
(+)-D-glucosamine hydrochloride

: 23661-45-2
2-phenyl-4,5-(5,6-isopropylidene-D-glucofurano)-1,3-oxazoline

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaOMe / methanol / 0.17 h

1.2: 91 percent / methanol / 0.5 h

2.1: FeCl₃ / 0.33 h / Heating

2.2: 79 percent / Et₂NH; aq. Na₂CO₃ / acetone / 0 °C

With sodium methylate; iron(III) chloride; In methanol;
DOI:10.1007/s00706-003-0086-1

Reference yield:

: 93-97-0
benzoic acid anhydride

: 23661-45-2
2-phenyl-4,5-(5,6-isopropylidene-D-glucofurano)-1,3-oxazoline

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaOMe / methanol / 0.17 h

1.2: 91 percent / methanol / 0.5 h

2.1: FeCl₃ / 0.33 h / Heating

2.2: 79 percent / Et₂NH; aq. Na₂CO₃ / acetone / 0 °C

With sodium methylate; iron(III) chloride; In methanol;
DOI:10.1007/s00706-003-0086-1