Bicyclo[3.1.0]hexan-3-one, 2-(1-hydroxyethylidene)-6,6-dimethyl-, (1S,2Z,5R)-

Base Information

• Chemical Name: Bicyclo[3.1.0]hexan-3-one, 2-(1-hydroxyethylidene)-6,6-dimethyl-, (1S,2Z,5R)-
• CAS No.: 340165-10-8
• Molecular Formula: C10H14O2
• Molecular Weight: 166.21696
• Mol file: 340165-10-8.mol

Synonyms:Bicyclo[3.1.0]hexan-3-one, 2-(1-hydroxyethylidene)-6,6-dimethyl-, (1S,2Z,5R)-

Chemical Property of Bicyclo[3.1.0]hexan-3-one, 2-(1-hydroxyethylidene)-6,6-dimethyl-, (1S,2Z,5R)-

Chemical Property:

• Boiling Point: 75 - 78 °C (2 - 3 mmHg)
• PSA: 37.30000
• LogP: 2.06340

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Bicyclo[3.1.0]hexan-3-one, 2-(1-hydroxyethylidene)-6,6-dimethyl-, (1S,2Z,5R)-

There total 2 articles about Bicyclo[3.1.0]hexan-3-one, 2-(1-hydroxyethylidene)-6,6-dimethyl-, (1S,2Z,5R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1-((1R,5R)-3-amino-6,6-dimethylbicyclo[3.1.0]hex-2-en-2-yl)ethanone (145696-98-6,313956-40-0) → (1R,5R)-6,6-dimethyl-2-(1-hydroxyethylidene)-bicyclo<3.1.0>hexan-3-one (340165-10-8)

Guidance literature:

With hydrogenchloride; In methanol; at 80 ℃; for 3h;

DOI:10.1016/S0957-4166(00)86220-5

Reference yield: 81.0%

2,2-dimethyl-3-(2-oxopropyl)-cis-cyclopropane-1-acetic acid methyl ester (54878-01-2) → (1R,5R)-6,6-dimethyl-2-(1-hydroxyethylidene)-bicyclo<3.1.0>hexan-3-one (340165-10-8)

Guidance literature:

With sodium methylate; In methanol; for 0.25h; Heating;

DOI:10.1016/S0957-4166(00)86220-5

Reference yield: 87.0%

phenylhydrazine (100-63-0) + (1R,5R)-6,6-dimethyl-2-(1-hydroxyethylidene)-bicyclo<3.1.0>hexan-3-one (340165-10-8) → (1S,8R)-5-phenyl-3,9,9-trimethyl-4,5-diazatricyclo[6.1.0.02,6]non-2(6),3-diene (156145-78-7)

Guidance literature:

With acetic acid; In methanol; for 8h; Heating;

DOI:10.1016/S0957-4166(00)86220-5

upstream raw materials:

2,2-dimethyl-3-(2-oxopropyl)-cis-cyclopropane-1-acetic acid methyl ester

1-((1R,5R)-3-amino-6,6-dimethylbicyclo[3.1.0]hex-2-en-2-yl)ethanone

Downstream raw materials:

(1S,8R)-5-phenyl-3,9,9-trimethyl-4,5-diazatricyclo[6.1.0.0^2,6]non-2⁽⁶⁾,3-diene

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