Cyclobutanecarboxylic acid, 3,3-diMethyl-, Methyl ester

Base Information

• Chemical Name: Cyclobutanecarboxylic acid, 3,3-diMethyl-, Methyl ester
• CAS No.: 3854-83-9
• Molecular Formula: C8H14O2
• Molecular Weight: 142.198
• Hs Code.: 2916209090
• Mol file: 3854-83-9.mol

Synonyms:Cyclobutanecarboxylic acid, 3,3-diMethyl-, Methyl ester;Methyl 3,3-diMethylcyclobutane-1-carboxylate;Methyl 3,3-dimethylcyclobutanecarboxylate

Chemical Property of Cyclobutanecarboxylic acid, 3,3-diMethyl-, Methyl ester

Chemical Property:

• PSA: 26.30000
• LogP: 1.59560

Purity/Quality:

99%, ^*data from raw suppliers

Methyl 3,3-dimethylcyclobutane-1-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of Cyclobutanecarboxylic acid, 3,3-diMethyl-, Methyl ester

There total 3 articles about Cyclobutanecarboxylic acid, 3,3-diMethyl-, Methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

3,3-dimethylcyclobutanecarboxylic acid (34970-18-8) + diazomethyl-trimethyl-silane (18107-18-1) → 3,3-dimethylcyclobutanecarboxylic acid methyl ester (3854-83-9)

Guidance literature:

With acetic acid; In methanol; acetonitrile;

Reference yield:

methyl (3,3-dimethyl-1-cyclobutene)carboxylate (37676-91-8) → 3,3-dimethylcyclobutanecarboxylic acid methyl ester (3854-83-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1021/ja01076a031

Reference yield:

N,N-diethylaniline (91-66-7) → 3,3-dimethylcyclobutanecarboxylic acid methyl ester (3854-83-9)

Guidance literature:

DOI:10.1039/jr9380001211

upstream raw materials:

methyl (3,3-dimethyl-1-cyclobutene)carboxylate

N,N-diethylaniline

3,3-dimethylcyclobutanecarboxylic acid

diazomethyl-trimethyl-silane

Downstream raw materials:

Diphenyl-<3,3-dimethyl-cyclobutyl>-carbinol

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