4-Hydroxy-3,5-diiodobenzaldehyde oxime

Base Information

• Chemical Name: 4-Hydroxy-3,5-diiodobenzaldehyde oxime
• CAS No.: 2296-76-6
• Molecular Formula: C7H5 I2 N O2
• Molecular Weight: 388.931
• Hs Code.: 2928000090
• Mol file: 2296-76-6.mol

Synonyms:3,5-Diiodo-4-hydroxybenzaldehyde,oxime; NSC 47954

Chemical Property of 4-Hydroxy-3,5-diiodobenzaldehyde oxime

Chemical Property:

• Vapor Pressure: 1.91E-05mmHg at 25°C
• Boiling Point: 324.5°Cat760mmHg
• Flash Point: 150°C
• PSA: 52.82000
• Density: 2.62g/cm³
• LogP: 2.40950

Purity/Quality:

99% ^*data from raw suppliers

3,5-DIIODO-4-HYDROXYBENZALDEHYDE OXIME 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Hydroxy-3,5-diiodobenzaldehyde oxime

There total 2 articles about 4-Hydroxy-3,5-diiodobenzaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

→ 4-hydroxy-3,5-diiodo-benzaldehyde-oxime (2296-76-6)

Guidance literature:

Reference yield:

4-hydroxy-3,5-diiodobenzaldehyde (1948-40-9) → 4-hydroxy-3,5-diiodo-benzaldehyde-oxime (2296-76-6)

Guidance literature:

With sodium hydroxide; hydroxylamine hydrochloride;

Reference yield:

4-hydroxy-3,5-diiodo-benzaldehyde-oxime (2296-76-6) + acetic anhydride (108-24-7) → 4-acetoxy-3,5-diiodo-benzonitrile (1689-85-6)

Guidance literature:

upstream raw materials:

4-hydroxy-3,5-diiodobenzaldehyde

Downstream raw materials:

4-[1-(4-Hydroxy-3,5-diiodo-phenyl)-meth-(Z)-ylideneaminooxy]-3-nitro-benzoic acid methyl ester

4-Hydroxy-3,5-diiodo-benzaldehyde O-(5-chloro-2,4-dinitro-phenyl)-oxime

4-[1-(4-Hydroxy-3,5-diiodo-phenyl)-meth-(Z)-ylideneaminooxy]-N,N-dimethyl-3-nitro-benzenesulfonamide

4-acetoxy-3,5-diiodo-benzonitrile

Refernces

• 1、 Lam, Patrick Y. S.,Adams, Jessica J.,Clark, Charles G.,Calhoun, W. Jason,Luettgen, Joseph M.,Knabb, Robert M.,Wexler, Ruth R.. "Discovery of 3-amino-4-chlorophenyl P1 as a novel and potent benzamidine mimic via solid-phase synthesis of an isoxazoline library". . p. 1795 - 1799. Retrieved 2007/10/03.