9-BENZYL-1-OXA-4,9-DIAZASPIRO[5.5]UNDECANE

Base Information

• Chemical Name: 9-BENZYL-1-OXA-4,9-DIAZASPIRO[5.5]UNDECANE
• CAS No.: 1018608-18-8
• Molecular Formula: C15H22N2O
• Molecular Weight: 246.352
• Mol file: 1018608-18-8.mol

Synonyms:9-BENZYL-1-OXA-4,9-DIAZASPIRO[5.5]UNDECANE;OTAVA-BB 1145935;9-(phenylmethyl)-1-Oxa-4,9-diazaspiro[5.5]undecane

Chemical Property of 9-BENZYL-1-OXA-4,9-DIAZASPIRO[5.5]UNDECANE

Chemical Property:

• PSA: 24.50000
• LogP: 1.90770

Purity/Quality:

NLT 98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 9-BENZYL-1-OXA-4,9-DIAZASPIRO[5.5]UNDECANE

There total 7 articles about 9-BENZYL-1-OXA-4,9-DIAZASPIRO[5.5]UNDECANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

tert-butyl 9-benzyl-1-oxa-4,9-diazaspiro[5.5]undecane-4-carboxylate → 9-benzyl-1-oxa-4,9-diazaspiro[5.5]undecane (1018608-18-8)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

9-benzyl-1-oxa-4,9-diazaspiro[5.5]undecan-3-one (1169699-64-2) → 9-benzyl-1-oxa-4,9-diazaspiro[5.5]undecane (1018608-18-8)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 0.666667h; Reflux;

Reference yield:

(2-{[(1-benzyl-4-hydroxypiperidin-4-yl)methyl]amino}ethoxy)sulfonic acid → 9-benzyl-1-oxa-4,9-diazaspiro[5.5]undecane (1018608-18-8)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; ethanol; for 5h; Reflux;

upstream raw materials:

1-phenylmethyl-4-piperidone

4-(aminomethyl)-1-benzyl-4-hydroxypiperidine

N-benzyl-1-oxa-6-azaspiro[2,5]-octane

9-benzyl-1-oxa-4,9-diazaspiro[5.5]undecan-3-one

Downstream raw materials:

C₂₂H₂₉N₃O₂S

C₁₅H₁₈F₂N₂O₂

C₂₃H₂₂F₅N₃O₄

C₁₆H₂₀F₃N₃O₂

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