Valine, 3-hydroxy-, ethyl ester (9CI)

Base Information

Chemical Name:Valine, 3-hydroxy-, ethyl ester (9CI)
CAS No.:738535-66-5
Molecular Formula:C7H15NO3
Molecular Weight:161.201
Hs Code.:
Mol file:738535-66-5.mol

Synonyms:Valine, 3-hydroxy-, ethyl ester (9CI)

Suppliers and Price of Valine, 3-hydroxy-, ethyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 2 raw suppliers

Chemical Property of Valine, 3-hydroxy-, ethyl ester (9CI)

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of Valine, 3-hydroxy-, ethyl ester (9CI)

There total 2 articles about Valine, 3-hydroxy-, ethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353743-41-5
ethyl 2-(((benzyloxy)carbonyl)amino)-3-hydroxy-3-methylbutanoate

: 738535-66-5
ethyl 2-amino-3-hydroxy-3-methylbutanoate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 23h; under 23272.3 Torr;
DOI:10.1021/jo202375a

Reference yield:

: 638-10-8
ethyl 3-methylbut-2-enoate

: 738535-66-5
ethyl 2-amino-3-hydroxy-3-methylbutanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: osmium(VIII) oxide / water; acetonitrile / 0.17 h / 20 °C

1.2: 10 h / 35 °C

2.1: palladium 10% on activated carbon; hydrogen / methanol / 23 h / 20 °C / 23272.3 Torr

With osmium(VIII) oxide; palladium 10% on activated carbon; hydrogen; In methanol; water; acetonitrile;
DOI:10.1021/jo202375a

Reference yield: 99.0%

: 738535-66-5
ethyl 2-amino-3-hydroxy-3-methylbutanoate

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 1353743-58-4
ethyl 2-(2-(((benzyloxy)carbonyl)amino)acetamido)-3-hydroxy-3-methylbutanoate

Guidance literature:: With sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 20 ℃; for 48h; Inert atmosphere;
DOI:10.1016/j.tetlet.2021.153175