2-chloro-3-(4-hydroxyphenyl)-1-propene

Base Information

• Chemical Name: 2-chloro-3-(4-hydroxyphenyl)-1-propene
• CAS No.: 13283-34-6
• Molecular Formula: C9H9 Cl O
• Molecular Weight: 168.623
• Hs Code.: 2908199090
• Mol file: 13283-34-6.mol

Synonyms:Phenol,4-(2-chloro-2-propenyl)- (9CI); Phenol, p-(2-chloroallyl)- (8CI);2-Chloro-3-(p-hydroxyphenyl)-1-propene

Chemical Property of 2-chloro-3-(4-hydroxyphenyl)-1-propene

Chemical Property:

• Vapor Pressure: 0.00286mmHg at 25°C
• Boiling Point: 276.4°C at 760 mmHg
• Flash Point: 121°C
• PSA: 20.23000
• Density: 1.175g/cm³
• LogP: 2.68720

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-chloro-3-(4-hydroxyphenyl)-1-propene

There total 2 articles about 2-chloro-3-(4-hydroxyphenyl)-1-propene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

2,3-Dichloroprop-1-ene (78-88-6) + 4-amino-phenol (123-30-8) → 4-(2-chloroallyl)phenol (13283-34-6) + phenol (108-95-2,27073-41-2)

Guidance literature:

4-amino-phenol; With hydrogenchloride; water; isopentyl nitrite;

2,3-Dichloroprop-1-ene; With ferrous(II) sulfate heptahydrate; dimethyl sulfoxide; In water; for 0.416667h;

DOI:10.1002/chem.201003713

Reference yield:

2,3-Dichloroprop-1-ene (78-88-6) + phenol (108-95-2,27073-41-2) → 4-(2-chloroallyl)phenol (13283-34-6)

Guidance literature:

With sodium phenoxide; at 165 - 170 ℃;

DOI:10.1021/jo01285a071

upstream raw materials:

2,3-Dichloroprop-1-ene

phenol

4-amino-phenol

Refernces