tert-butyl 4-oxotetrahydrofuran-3-ylcarbaMate

Base Information

Chemical Name:tert-butyl 4-oxotetrahydrofuran-3-ylcarbaMate
CAS No.:1414975-77-1
Molecular Formula:C9H15NO4
Molecular Weight:201.2197
Hs Code.:
Mol file:1414975-77-1.mol

Synonyms:tert-butyl 4-oxotetrahydrofuran-3-ylcarbaMate;tert-butyl tetrahydro-4-oxofuran-3-ylcarbamate

Suppliers and Price of tert-butyl 4-oxotetrahydrofuran-3-ylcarbaMate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Tert-ButylN-(4-Oxooxolan-3-Yl)Carbamate
50mg
$ 220.00

Crysdot
tert-Butyl(4-oxotetrahydrofuran-3-yl)carbamate 95+%
1g
$ 913.00

Chemenu
tert-Butyl(4-oxotetrahydrofuran-3-yl)carbamate 95%
1g
$ 861.00

aablocks
tert-Butyln-(4-oxooxolan-3-yl)carbamate 95%
100mg
$ 176.00

aablocks
tert-Butyln-(4-oxooxolan-3-yl)carbamate 95%
1g
$ 607.00

aablocks
tert-Butyln-(4-oxooxolan-3-yl)carbamate 95%
250mg
$ 304.00

Total 2 raw suppliers

Chemical Property of tert-butyl 4-oxotetrahydrofuran-3-ylcarbaMate

Chemical Property:

PSA：64.63000
LogP:0.86990

Purity/Quality:

99% ^*data from raw suppliers

Tert-ButylN-(4-Oxooxolan-3-Yl)Carbamate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of tert-butyl 4-oxotetrahydrofuran-3-ylcarbaMate

There total 2 articles about tert-butyl 4-oxotetrahydrofuran-3-ylcarbaMate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1430230-65-1,412278-24-1
(±)-trans-3-tert-butoxycarbonylamino-4-hydroxytetrahydrofuran

: 1414975-77-1,406220-17-5
tert-butyl N-(4-oxotetrahydrofuran-3-yl)carbamate

Guidance literature:: (±)-trans-3-tert-butoxycarbonylamino-4-hydroxytetrahydrofuran; With oxalyl dichloride; dimethyl sulfoxide; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

With triethylamine; In tetrahydrofuran; at -78 - 20 ℃; for 16h;

Reference yield:

: 1708-29-8
2,5-dihydrofuran

: 24424-99-5
di-tert-butyl dicarbonate

: 1414975-77-1,406220-17-5
tert-butyl N-(4-oxotetrahydrofuran-3-yl)carbamate

Guidance literature:: 2,5-dihydrofuran; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃;

With sodium azide; ammonium chloride; In methanol; water; Reflux;

di-tert-butyl dicarbonate; Further stages;
DOI:10.1007/s12039-020-01833-x