3-phenyl-7H-benzo[de]anthracen-7-one

Base Information

• Chemical Name: 3-phenyl-7H-benzo[de]anthracen-7-one
• CAS No.: 18792-80-8
• Molecular Formula: C23H14O
• Molecular Weight: 306.364
• NSC Number: 176040
• DSSTox Substance ID: DTXSID10306388
• Nikkaji Number: J82.801G
• Wikidata: Q82053469
• Mol file: 18792-80-8.mol

Synonyms:3-phenylbenzo[b]phenalen-7-one;18792-80-8;3-Phenyl-7H-benz[de]anthracen-7-one;3-phenyl-7H-benzo[de]anthracen-7-one;3-phenylbenzanthrone;NSC176040;SCHEMBL24334669;DTXSID10306388;XPUFZUYCTSSNTI-UHFFFAOYSA-N;NSC-176040;7H-Benz[de]anthracen-7-one, 3-phenyl-

Chemical Property of 3-phenyl-7H-benzo[de]anthracen-7-one

Chemical Property:

• Vapor Pressure: 1.02E-10mmHg at 25°C
• Boiling Point: 515°C at 760 mmHg
• Flash Point: 228.8°C
• PSA: 17.07000
• Density: 1.254g/cm³
• LogP: 5.71820
• XLogP3: 5.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 306.104465066
• Heavy Atom Count: 24
• Complexity: 476

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C2=C3C=CC=C4C3=C(C=C2)C5=CC=CC=C5C4=O

Technology Process of 3-phenyl-7H-benzo[de]anthracen-7-one

There total 27 articles about 3-phenyl-7H-benzo[de]anthracen-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

3-phenyl-2-(tributylstannyl)-7H-benzo[de]anthracen-7-one → 1-phenylbenzanthrone (18792-80-8)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 23 ℃; for 0.0833333h; Inert atmosphere;

DOI:10.1002/anie.201712783

Reference yield: 67.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + anthracen-9(10H)-one (90-44-8) → 1-phenylbenzanthrone (18792-80-8)

Guidance literature:

DOI:10.1134/S107042801006014X

Reference yield:

(E)-3-phenylpropenal (14371-10-9) + anthracen-9(10H)-one (90-44-8) → 1-phenylbenzanthrone (18792-80-8)

Guidance literature:

With 1-Chloronaphthalene; at 250 - 260 ℃;

DOI:10.1080/00049530108255130

upstream raw materials:

styrene

formaldehyd

anthracen-9(10H)-one

10-Methylene-10H-anthracen-9-one

Downstream raw materials:

6-ethyl-3-phenyl-benz[de]anthracen-7-one

6-hexyl-3-phenyl-benz[de]anthracen-7-one

2-phenyl-benz[de]anthracen-7-one

1-benzoylanthraquinone