1,1,3-Cyclobutanetricarboxylicacid,3-amino-(9CI)

Base Information

Chemical Name:1,1,3-Cyclobutanetricarboxylicacid,3-amino-(9CI)
CAS No.:129287-89-4
Molecular Formula:C7H9NO6
Molecular Weight:203.14946
Hs Code.:
Mol file:129287-89-4.mol

Synonyms:1,1,3-Cyclobutanetricarboxylicacid,3-amino-(9CI)

Suppliers and Price of 1,1,3-Cyclobutanetricarboxylicacid,3-amino-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1,3-Cyclobutanetricarboxylicacid,3-amino-(9CI)

Chemical Property:

PSA：137.92000
LogP:-0.58180

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,1,3-Cyclobutanetricarboxylicacid,3-amino-(9CI)

There total 5 articles about 1,1,3-Cyclobutanetricarboxylicacid,3-amino-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54166-15-3
diethyl 3-(benzyloxy)cyclobutane-1,1-dicarboxylate

: 129287-89-4
3-aminocyclobutane-1,1,3-tricarboxylic acid

Guidance literature:: Multi-step reaction with 5 steps

1: H₂ / 10percent Pd/C / ethanol / 760 Torr

2: 92 percent / sodium metaperiodate, RuO₄ / H₂O; CCl₄ / 24 h

3: aq. KOH / ethanol

4: concd. NH₄OH, NH₄HCO₃*NH₂CO₂NH₄, NH₄Cl / methanol; H₂O / 3 h / Heating

5: 0.5 M aq. NaOH / Heating

With potassium hydroxide; ammonium hydroxide; sodium hydroxide; sodium periodate; ruthenium tetroxide; hydrogen; ammonium carbamate; ammonium bicarbonate; ammonium chloride; palladium on activated charcoal; In methanol; tetrachloromethane; ethanol; water;
DOI:10.1021/jm00172a036

Reference yield:

: 99974-66-0
diethyl 3-hydroxycyclobutane-1,1-dicarboxylate

: 129287-89-4
3-aminocyclobutane-1,1,3-tricarboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / sodium metaperiodate, RuO₄ / H₂O; CCl₄ / 24 h

2: aq. KOH / ethanol

3: concd. NH₄OH, NH₄HCO₃*NH₂CO₂NH₄, NH₄Cl / methanol; H₂O / 3 h / Heating

4: 0.5 M aq. NaOH / Heating

With potassium hydroxide; ammonium hydroxide; sodium hydroxide; sodium periodate; ruthenium tetroxide; ammonium carbamate; ammonium bicarbonate; ammonium chloride; In methanol; tetrachloromethane; ethanol; water;
DOI:10.1021/jm00172a036

Reference yield:

: 99173-61-2
diethyl 3-oxo-cyclobutane-1,1-dicarboxylate

: 129287-89-4
3-aminocyclobutane-1,1,3-tricarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: aq. KOH / ethanol

2: concd. NH₄OH, NH₄HCO₃*NH₂CO₂NH₄, NH₄Cl / methanol; H₂O / 3 h / Heating

3: 0.5 M aq. NaOH / Heating

With potassium hydroxide; ammonium hydroxide; sodium hydroxide; ammonium carbamate; ammonium bicarbonate; ammonium chloride; In methanol; ethanol; water;
DOI:10.1021/jm00172a036