5-bromo-3-(phthalimidomethyl)pyridine

Base Information

Chemical Name:5-bromo-3-(phthalimidomethyl)pyridine
CAS No.:219660-71-6
Molecular Formula:C₁₄H₉BrN₂O₂
Molecular Weight:317.142
Hs Code.:2933399090
Mol file:219660-71-6.mol

Synonyms:5-bromo-3-(phthalimidomethyl)pyridine;2-((5-bromopyridin-3-yl)methyl)isoindoline-1,3-dione

Suppliers and Price of 5-bromo-3-(phthalimidomethyl)pyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Labseeker
2-((5-bromopyridin-3-yl)methyl)isoindoline-1,3-dione 95
2g
$ 1217.00

Crysdot
2-((5-Bromopyridin-3-yl)methyl)isoindoline-1,3-dione 95+%
1g
$ 377.00

Chemenu
2-((5-bromopyridin-3-yl)methyl)isoindoline-1,3-dione 95%
1g
$ 356.00

American Custom Chemicals Corporation
2-((5-BROMOPYRIDIN-3-YL)METHYL)ISOINDOLINE-1,3-DIONE 95.00%
5MG
$ 503.99

Alichem
2-((5-Bromopyridin-3-yl)methyl)isoindoline-1,3-dione
1g
$ 400.00

Total 9 raw suppliers

Chemical Property of 5-bromo-3-(phthalimidomethyl)pyridine

Chemical Property:

PSA：50.27000
LogP:2.57820
Storage Temp.:2-8°C

Purity/Quality:

99% ^*data from raw suppliers

2-((5-bromopyridin-3-yl)methyl)isoindoline-1,3-dione 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-bromo-3-(phthalimidomethyl)pyridine

There total 4 articles about 5-bromo-3-(phthalimidomethyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 136918-14-4,85-41-6
phthalimide

: 37669-64-0
(5-bromopyridin-3-yl)methanol

: 219660-71-6
2-((5-bromopyridin-3-yl)methyl)isoindoline-1,3-dione

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jo800028q

Reference yield:

: 135124-70-8
(5-bromo-3-pyridinyl)methylamine

: 219660-71-6
2-((5-bromopyridin-3-yl)methyl)isoindoline-1,3-dione

Guidance literature:

Reference yield:

: 113118-81-3
5-bromopyridine-3-carbaldehyde

: 219660-71-6
2-((5-bromopyridin-3-yl)methyl)isoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 2 h / 0 - 20 °C

2: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / tetrahydrofuran / 6 h / 20 °C

With sodium tetrahydroborate; tributylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; methanol;