3-(Aminomethyl)-5-bromopyridine 97%

Base Information

• Chemical Name: 3-(Aminomethyl)-5-bromopyridine 97%
• CAS No.: 135124-70-8
• Molecular Formula: C6H7BrN2
• Molecular Weight: 187.04
• Hs Code.: 2933399990
• Mol file: 135124-70-8.mol

Synonyms:3-(Aminomethyl)-5-bromopyridine 97%;(5-BROMO-3-PYRIDINYL)METHYLAMINE;5-BROMO-3-PYRIDINEMETHANAMINE;5-BROMO-3-PYRIDINEMETHYLAMINE;3-(Aminomethyl)-5-bromopyridine

Chemical Property of 3-(Aminomethyl)-5-bromopyridine 97%

Chemical Property:

• Vapor Pressure: 0.00726mmHg at 25°C
• Refractive Index: 1.596
• Boiling Point: 269.4°Cat760mmHg
• PKA: 7.75±0.29(Predicted)
• Flash Point: 116.7°C
• PSA: 38.91000
• Density: 1.574g/cm³
• LogP: 2.00310
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

>=98% ^*data from raw suppliers

3-(Aminomethyl)-5-bromopyridine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: C

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(Aminomethyl)-5-bromopyridine 97%

There total 16 articles about 3-(Aminomethyl)-5-bromopyridine 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.7%

2-((5-bromopyridin-3-yl)methyl)isoindoline-1,3-dione (219660-71-6) → (5-bromo-3-pyridinyl)methylamine (135124-70-8)

Guidance literature:

With hydrazine hydrate; In ethanol; at 70 ℃; for 3h;

Reference yield: 88.0%

3-bromo-5-(N,N-bis-tert-butoxycarbonyl)aminomethylpyridine (375854-08-3) → (5-bromo-3-pyridinyl)methylamine (135124-70-8)

Guidance literature:

3-bromo-5-(N,N-bis-tert-butoxycarbonyl)aminomethylpyridine; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

With Amberlite IRA-400(OH); In methanol; for 2h;

Reference yield: 88.0%

→ (5-bromo-3-pyridinyl)methylamine (135124-70-8)

Guidance literature:

upstream raw materials:

3-bromo-5-(N,N-bis-tert-butoxycarbonyl)aminomethylpyridine

phthalimide

(5-bromopyridin-3-yl)methanol

5-bromonicotinamide

Downstream raw materials:

N-[(5-Bromopyridin-3-yl)methyl]-10-[(2'-methoxy-1,1'-biphenyl-4-yl)carbonyl]-10,11-dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepine-3-carboxamide

1-(5-bromopyridin-3-yl)-N-(diphenylmethylene)methanamine

3-bromo-5-(tert-butoxycarbonyl)aminomethylpyridine