Trichloro-N-[(nonafluorobutyl)sulfinyl]phosphine imide

Base Information

• Chemical Name: Trichloro-N-[(nonafluorobutyl)sulfinyl]phosphine imide
• CAS No.: 51735-88-7
• Molecular Formula: C8H12F9NOSSi
• Molecular Weight: 418.434
• Hs Code.: 2931900090
• Mol file: 51735-88-7.mol

Synonyms:Trichloro-N-[(nonafluorobutyl)sulfinyl]phosphine imide

Chemical Property of Trichloro-N-[(nonafluorobutyl)sulfinyl]phosphine imide

Chemical Property:

• PSA: 39.52000
• LogP: 4.70820

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Trichloro-N-[(nonafluorobutyl)sulfinyl]phosphine imide

There total 2 articles about Trichloro-N-[(nonafluorobutyl)sulfinyl]phosphine imide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

phosphorus pentachloride (10026-13-8,874483-75-7) + N-trimethylsilyl-nonafluorobutanesulfinamide (51735-80-9) → N-(trichlorophosphoranylidene)-n-nonafluorobutanesulfinamide (51735-88-7)

Guidance literature:

In dichloromethane; reflux 0.5 h;

Reference yield:

N-trimethylsilyl-nonafluorobutanesulfinamide (51735-80-9) → N-(trichlorophosphoranylidene)-n-nonafluorobutanesulfinamide (51735-88-7)

Guidance literature:

With phosphorus trichloride; In dichloromethane;

Reference yield:

N-(trichlorophosphoranylidene)-n-nonafluorobutanesulfinamide (51735-88-7) → 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine (940-71-6,16422-79-0) + nonafluorobutanesulfinyl chloride (41006-41-1)

Guidance literature:

thermolysis at 120°C, 24 h;

upstream raw materials:

N-trimethylsilyl-nonafluorobutanesulfinamide

phosphorus pentachloride

Downstream raw materials:

2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine

nonafluorobutanesulfinyl chloride

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