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alpha-L-Ribofuranose 1,3,5-tribenzoate 2-(1H-imidazole-1-sulfonate)

Base Information Edit
  • Chemical Name:alpha-L-Ribofuranose 1,3,5-tribenzoate 2-(1H-imidazole-1-sulfonate)
  • CAS No.:171720-99-3
  • Molecular Formula:C29H24N2O10S
  • Molecular Weight:592.583
  • Hs Code.:
  • Mol file:171720-99-3.mol
alpha-L-Ribofuranose 1,3,5-tribenzoate 2-(1H-imidazole-1-sulfonate)

Synonyms:alpha-L-Ribofuranose 1,3,5-tribenzoate 2-(1H-imidazole-1-sulfonate)

Suppliers and Price of alpha-L-Ribofuranose 1,3,5-tribenzoate 2-(1H-imidazole-1-sulfonate)
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
Total 2 raw suppliers
Chemical Property of alpha-L-Ribofuranose 1,3,5-tribenzoate 2-(1H-imidazole-1-sulfonate) Edit
Chemical Property:
Purity/Quality:

≥95% *data from raw suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
Technology Process of alpha-L-Ribofuranose 1,3,5-tribenzoate 2-(1H-imidazole-1-sulfonate)

There total 18 articles about alpha-L-Ribofuranose 1,3,5-tribenzoate 2-(1H-imidazole-1-sulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 6 steps
1: 98 percent / pyridine / 3 h / Ambient temperature
2: 1percent HCl / methanol / 30 h / Ambient temperature
3: pyridine / 3 h / Ambient temperature
4: AcOH, conc. H2SO4 / Ambient temperature
5: 1.) HCl(g), AcCl, 2.) H2O / 1.) CH2Cl2, 0 deg C, 2.) CH3CN
6: 1.) SO2Cl2 / 1.) CH2Cl2, DMF, from -40 deg C to RT, 3.5 h, 2.) CH2Cl2, DMF, RT, 15 h
With pyridine; hydrogenchloride; sulfuryl dichloride; sulfuric acid; water; acetic acid; acetyl chloride; In methanol;
DOI:10.1021/jm960098l
Guidance literature:
Multi-step reaction with 7 steps
1: 79 percent / NaBH4, H2O / ethanol / 4 h / Ambient temperature
2: 98 percent / pyridine / 3 h / Ambient temperature
3: 1percent HCl / methanol / 30 h / Ambient temperature
4: pyridine / 3 h / Ambient temperature
5: AcOH, conc. H2SO4 / Ambient temperature
6: 1.) HCl(g), AcCl, 2.) H2O / 1.) CH2Cl2, 0 deg C, 2.) CH3CN
7: 1.) SO2Cl2 / 1.) CH2Cl2, DMF, from -40 deg C to RT, 3.5 h, 2.) CH2Cl2, DMF, RT, 15 h
With pyridine; hydrogenchloride; sodium tetrahydroborate; sulfuryl dichloride; sulfuric acid; water; acetic acid; acetyl chloride; In methanol; ethanol;
DOI:10.1021/jm960098l
Guidance literature:
Multi-step reaction with 8 steps
1: 96 percent / pyridinium dichromate, Ac2O / CH2Cl2 / 1.5 h / Heating
2: 79 percent / NaBH4, H2O / ethanol / 4 h / Ambient temperature
3: 98 percent / pyridine / 3 h / Ambient temperature
4: 1percent HCl / methanol / 30 h / Ambient temperature
5: pyridine / 3 h / Ambient temperature
6: AcOH, conc. H2SO4 / Ambient temperature
7: 1.) HCl(g), AcCl, 2.) H2O / 1.) CH2Cl2, 0 deg C, 2.) CH3CN
8: 1.) SO2Cl2 / 1.) CH2Cl2, DMF, from -40 deg C to RT, 3.5 h, 2.) CH2Cl2, DMF, RT, 15 h
With pyridine; hydrogenchloride; sodium tetrahydroborate; dipyridinium dichromate; sulfuryl dichloride; sulfuric acid; water; acetic anhydride; acetic acid; acetyl chloride; In methanol; ethanol; dichloromethane;
DOI:10.1021/jm960098l
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