Methyl 4-amino-3-fluoro-5-iodobenzoate

Base Information

• Chemical Name: Methyl 4-amino-3-fluoro-5-iodobenzoate
• CAS No.: 1123172-01-9
• Molecular Formula: C8H7FINO2
• Molecular Weight: 295.052
• Hs Code.: 2922499990
• Mol file: 1123172-01-9.mol

Synonyms:Methyl 4-amino-3-fluoro-5-iodobenzoate;2-Fluoro-6-iodo-4-(methoxycarbonyl)aniline;Methyl 4-amino-3-fluoro-5-iodobenzoate 95+%

Chemical Property of Methyl 4-amino-3-fluoro-5-iodobenzoate

Chemical Property:

• PSA: 52.32000
• LogP: 2.38030
• Storage Temp.: 2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

Methyl 4-amino-3-fluoro-5-iodobenzoate >95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 4-amino-3-fluoro-5-iodobenzoate

There total 2 articles about Methyl 4-amino-3-fluoro-5-iodobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.593%

methyl 4-amino-3-fluorobenzene carboxylate (185629-32-7) → 4-amino-3-fluoro-5-iodobenzoic acid methyl ester (1123172-01-9)

Guidance literature:

With N-iodo-succinimide; at 20 ℃;

Reference yield:

4-amino-3-fluorobenzoic acid (455-87-8) → 4-amino-3-fluoro-5-iodobenzoic acid methyl ester (1123172-01-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydrogencarbonate; sulfuric acid / 12 h / 80 °C

2: calcium carbonate / water / 36 h / 25 °C

With sulfuric acid; sodium hydrogencarbonate; calcium carbonate; In water;

Reference yield: 86.0%

4-amino-3-fluoro-5-iodobenzoic acid methyl ester (1123172-01-9) → C7H5FINO2

Guidance literature:

With sodium hydroxide; In ethanol; for 2h; Reflux;

upstream raw materials:

methyl 4-amino-3-fluorobenzene carboxylate

4-amino-3-fluorobenzoic acid

Downstream raw materials:

4-amino-3-but-1-ynyl-5-fluoro-benzoic acid methyl ester

4-amino-3-fluoro-5-iodo-benzonitrile

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