5-Acetyl-3-bromo-6-[(E)-2-(dimethylamino)ethenyl]-2(1H)-pyridinone

Base Information

Chemical Name:5-Acetyl-3-bromo-6-[(E)-2-(dimethylamino)ethenyl]-2(1H)-pyridinone
CAS No.:147293-24-1
Molecular Formula:C₁₁H₁₃BrN₂O₂
Molecular Weight:285.14
Hs Code.:2933399090
Mol file:147293-24-1.mol

Synonyms:5-Acetyl-3-bromo-6-[(E)-2-(dimethylamino)ethenyl]-2(1H)-pyridinone

Suppliers and Price of 5-Acetyl-3-bromo-6-[(E)-2-(dimethylamino)ethenyl]-2(1H)-pyridinone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
5-Acetyl-3-bromo-6-[(E)-2-(dimethylamino)ethenyl]-2(1H)-pyridinone >95%
500mg
$ 599.00

Crysdot
(E)-5-Acetyl-3-bromo-6-(2-(dimethylamino)vinyl)pyridin-2(1H)-one 95+%
1g
$ 630.00

AK Scientific
5-Acetyl-3-bromo-6-[(E)-2-(dimethylamino)ethenyl]-2(1H)-pyridinone
500mg
$ 858.00

Total 2 raw suppliers

Chemical Property of 5-Acetyl-3-bromo-6-[(E)-2-(dimethylamino)ethenyl]-2(1H)-pyridinone

Chemical Property:

Melting Point:236-238(dec)°
PSA：53.43000
LogP:2.28460

Purity/Quality:

99% ^*data from raw suppliers

5-Acetyl-3-bromo-6-[(E)-2-(dimethylamino)ethenyl]-2(1H)-pyridinone >95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-Acetyl-3-bromo-6-[(E)-2-(dimethylamino)ethenyl]-2(1H)-pyridinone

There total 2 articles about 5-Acetyl-3-bromo-6-[(E)-2-(dimethylamino)ethenyl]-2(1H)-pyridinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 5815-08-7
tert-Butoxybis(dimethylamino)methane

: 136117-46-9
5-acetyl-3-bromo-6-methyl-2(1H)-pyridinone

: 147293-24-1
5-acetyl-3-bromo-6-<2-(dimethylamino)ethenyl>pyridin-2(1H)-one

Guidance literature:: In 1,4-dioxane; for 5h; Heating;
DOI:10.3987/COM-92-6193

Reference yield:

: 5220-65-5
5-acetyl-6-methyl-2(1H)-pyridinone

: 147293-24-1
5-acetyl-3-bromo-6-<2-(dimethylamino)ethenyl>pyridin-2(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / NBS, benzoyl peroxide / CCl₄ / 8 h / Heating

2: 90 percent / dioxane / 5 h / Heating

With N-Bromosuccinimide; Perbenzoic acid; In 1,4-dioxane; tetrachloromethane;
DOI:10.3987/COM-92-6193