N-Hydrazinocarbonylmethyl-3,4,5-trimethoxy-benzamide

Base Information

Chemical Name:N-Hydrazinocarbonylmethyl-3,4,5-trimethoxy-benzamide
CAS No.:63203-45-2
Molecular Formula:C12H17N3O5
Molecular Weight:283.284
Hs Code.:
NSC Number:39074
DSSTox Substance ID:DTXSID20284800
Wikidata:Q82019930
ChEMBL ID:CHEMBL570136

Synonyms:63203-45-2;N-Hydrazinocarbonylmethyl-3,4,5-trimethoxy-benzamide;NSC39074;N-(2-hydrazinyl-2-oxoethyl)-3,4,5-trimethoxybenzamide;Oprea1_314221;Oprea1_339919;CHEMBL570136;SCHEMBL17038616;DTXSID20284800;NSC-39074;STL193512;AKOS000518482;CS-0331539;A1-04862;N-Hydrazinocarbonylmethyl-3,4,5-trimethoxybenzamide;N-(2-hydrazino-2-oxo-ethyl)-3,4,5-trimethoxy-benzamide;N-[(HYDRAZINECARBONYL)METHYL]-3,4,5-TRIMETHOXYBENZAMIDE;N-(2-hydrazinyl-2-oxoethyl)-3,4,5-trimethoxybenzamide (non-preferred name)

Suppliers and Price of N-Hydrazinocarbonylmethyl-3,4,5-trimethoxy-benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of N-Hydrazinocarbonylmethyl-3,4,5-trimethoxy-benzamide

Chemical Property:

Vapor Pressure:3.17E-09mmHg at 25°C
Boiling Point:476°Cat760mmHg
Flash Point:241.7°C
Density:1.242g/cm³
XLogP3:-0.3
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:6
Exact Mass:283.11682065
Heavy Atom Count:20
Complexity:325

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=CC(=C1OC)OC)C(=O)NCC(=O)NN

Technology Process of N-Hydrazinocarbonylmethyl-3,4,5-trimethoxy-benzamide

There total 4 articles about N-Hydrazinocarbonylmethyl-3,4,5-trimethoxy-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.6%

: 92502-39-1
ethyl ((3,4,5-trimethoxybenzoyl)amino)acetate

: 63203-45-2
N-(2-hydrazino-2-oxoethyl)-3,4,5-trimethoxybenzamide

Guidance literature:: With hydrazine hydrate; In ethanol; at 80 ℃; for 15h;

Reference yield:

: 118-41-2
Eudesmic acid

: 63203-45-2
N-(2-hydrazino-2-oxoethyl)-3,4,5-trimethoxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride / N,N-dimethylformamide / CH₂Cl₂

2: 1.83 g / N-ethyl-N,N-diisopropylamine / CH₂Cl₂

3: 72 percent / hydrazine hydrate / ethanol / 24 h / Heating

With oxalyl dichloride; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In ethanol; dichloromethane;
DOI:10.1021/jm060742o

Reference yield:

: 4521-61-3
3,4,5-Trimethoxybenzoyl chloride

: 63203-45-2
N-(2-hydrazino-2-oxoethyl)-3,4,5-trimethoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.83 g / N-ethyl-N,N-diisopropylamine / CH₂Cl₂

2: 72 percent / hydrazine hydrate / ethanol / 24 h / Heating

With hydrazine hydrate; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane;
DOI:10.1021/jm060742o