E-2-(3,5-DIMETHOXYPHENYL)VINYLBORONIC ACID PINACOL ESTER

Base Information

Chemical Name:E-2-(3,5-DIMETHOXYPHENYL)VINYLBORONIC ACID PINACOL ESTER
CAS No.:1073354-86-5
Molecular Formula:C16H25BO5
Molecular Weight:290.167
Hs Code.:2934999090
ChEMBL ID:CHEMBL2315712
DSSTox Substance ID:DTXSID60584811
Wikidata:Q82476542
Mol file:1073354-86-5.mol

Synonyms:TRANS-2-(3,5-DIMETHOXYPHENYL)VINYLBORONIC ACID PINACOL ESTER;E-2-(3,5-DIMETHOXYPHENYL)VINYLBORONIC ACID PINACOL ESTER;(E)-2-(3,5-DiMethoxystyryl)-4,4,5,5-tetraMethyl-1,3,2-dioxaborolane;2-[(1E)-2-(3,5-Dimethoxyphenyl)ethenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane;trans-2-(3,5-Dimethoxyphenyl)vinylboronic acid pinacol ester 97%

Suppliers and Price of E-2-(3,5-DIMETHOXYPHENYL)VINYLBORONIC ACID PINACOL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
E-2-(3,5-Dimethoxyphenyl)vinylboronicacidpinacolester
250mg
$ 165.00

Sigma-Aldrich
trans-2-(3,5-Dimethoxyphenyl)vinylboronic acid pinacol ester 97%
1g
$ 158.00

Crysdot
(E)-2-(3,5-Dimethoxystyryl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 95+%
5g
$ 662.00

Chemenu
(E)-2-(3,5-Dimethoxystyryl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 95%
1g
$ 105.00

American Custom Chemicals Corporation
TRANS-2-(3,5-DIMETHOXYPHENYL)VINYLBORONIC ACID PINACOL ESTER 95.00%
1G
$ 401.10

Alichem
(E)-2-(3,5-Dimethoxystyryl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
1g
$ 400.00

Total 16 raw suppliers

Chemical Property of E-2-(3,5-DIMETHOXYPHENYL)VINYLBORONIC ACID PINACOL ESTER

Chemical Property:

Melting Point:56-62 °C
PSA：36.92000
LogP:3.34840
Storage Temp.:2-8°C
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:290.1689394
Heavy Atom Count:21
Complexity:353

Purity/Quality:

97% ^*data from raw suppliers

E-2-(3,5-Dimethoxyphenyl)vinylboronicacidpinacolester ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B1(OC(C(O1)(C)C)(C)C)C=CC2=CC(=CC(=C2)OC)OC
Isomeric SMILES:B1(OC(C(O1)(C)C)(C)C)/C=C/C2=CC(=CC(=C2)OC)OC

Technology Process of E-2-(3,5-DIMETHOXYPHENYL)VINYLBORONIC ACID PINACOL ESTER

There total 3 articles about E-2-(3,5-DIMETHOXYPHENYL)VINYLBORONIC ACID PINACOL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 171290-52-1
1-Ethynyl-3,5-dimethoxy-benzene

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1073354-86-5
2-[(E)-2-(3,5-dimethoxyphenyl)vinyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With silver hexafluoroantimonate; In neat (no solvent); at 20 ℃; for 48h; stereoselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1039/c8cc07499b

Reference yield: 78.1%

: 20469-65-2
1-bromo-3,5-dimethoxybenzene

: 75927-49-0
pinacol vinylboronate

: 1073354-86-5
2-[(E)-2-(3,5-dimethoxyphenyl)vinyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine; tri tert-butylphosphoniumtetrafluoroborate; In toluene; at 95 ℃; for 6h; Inert atmosphere;
DOI:10.1039/d1ra01147b

Reference yield: 64.0%

: C₁₁H₁₄O₃

: 73183-34-3
bis(pinacol)diborane

: 1073354-86-5
2-[(E)-2-(3,5-dimethoxyphenyl)vinyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With bis(acetylacetonate)nickel(II); potassium phosphate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; zinc; In cyclohexane; toluene; at 120 ℃; for 24h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.0c02236