1-Amino-3-methyl-butan-2-ol

Base Information

• Chemical Name: 1-Amino-3-methyl-butan-2-ol
• CAS No.: 17687-58-0
• Molecular Formula: C₅H₁₃NO
• Molecular Weight: 103.164
• Hs Code.: 2922199090
• Mol file: 17687-58-0.mol

Synonyms:1-Amino-3-methyl-butan-2-ol;MFCD09260580;1-Amino-3-methyl-2-butanol HCl

Chemical Property of 1-Amino-3-methyl-butan-2-ol

Chemical Property:

• Melting Point: 26-27 °C
• Boiling Point: 174 °C(Press: 764 Torr)
• PKA: 12.78±0.35(Predicted)
• PSA: 46.25000
• Density: 0.912±0.06 g/cm3(Predicted)
• LogP: 0.66230

Purity/Quality:

97% ^*data from raw suppliers

1-Amino-3-methylbutan-2-ol 95%+ ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Amino-3-methyl-butan-2-ol

There total 9 articles about 1-Amino-3-methyl-butan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

Benzyl-(2-hydroxy-3-methyl-butyl)-carbamic acid benzyl ester (123933-99-3) → 1-amino-3-methylbutan-2-ol (17687-58-0,208850-56-0)

Guidance literature:

With ammonium formate; palladium on activated charcoal; In methanol; for 1.5h; Heating;

DOI:10.1021/jo00285a005

Reference yield: 84.0%

3-methyl-1-nitrobutan-2-ol (141377-55-1,141434-98-2,2224-38-6) → 1-amino-3-methylbutan-2-ol (17687-58-0,208850-56-0)

Guidance literature:

With indium; acetic acid; In tetrahydrofuran; for 50h; Heating;

DOI:10.1039/b101712h

Reference yield:

2-isopropyloxirane (1438-14-8) → 1-amino-3-methylbutan-2-ol (17687-58-0,208850-56-0)

Guidance literature:

With ammonium hydroxide; In ethanol;

DOI:10.1021/jo01013a046

upstream raw materials:

3-methyl-1-nitrobutan-2-ol

2-isopropyloxirane

2-acetoxyisovaleronitrile

hydrogen cyanide

Downstream raw materials:

3-methyl-butan-2-one

N-{(3R,6S)-6-(2,3-difluorophenyl)-2-[(2-hydroxy-3-methylbutyl)imino]azepan}-4-(2-oxo-2,3-dihydro-1H-imidazo[4,5-b]pyridin-1-yl)piperidine-1-carboxamide

(±)-tert-butyl (2-hydroxy-3-methylbutyl)carbamate

C₂₂H₂₉F₂N₃O₂

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