2-(2-METHOXYPHENOXY)BENZOIC ACID

Base Information

• Chemical Name: 2-(2-METHOXYPHENOXY)BENZOIC ACID
• CAS No.: 21905-73-7
• Molecular Formula: C14H12O4
• Molecular Weight: 244.247
• Hs Code.: 2918990090
• Mol file: 21905-73-7.mol

Synonyms:2-(2-METHOXYPHENOXY)BENZOIC ACID;AKOS BBS-00001148;Benzoic acid, 2-(2-methoxyphenoxy)-;Benzoic acid, o-(o-methoxyphenoxy)-

Chemical Property of 2-(2-METHOXYPHENOXY)BENZOIC ACID

Chemical Property:

• PSA: 55.76000
• LogP: 3.18570
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

2-(2-Methoxyphenoxy)benzoic acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(2-METHOXYPHENOXY)BENZOIC ACID

There total 15 articles about 2-(2-METHOXYPHENOXY)BENZOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

2-Iodobenzoic acid (88-67-5) + 2-methoxy-phenol (90-05-1) → 2-carboxy-2'-methoxydiphenyl ether (21905-73-7)

Guidance literature:

With pyridine; copper(l) iodide; copper; 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 160 ℃; Inert atmosphere;

DOI:10.1039/c6ob01758d

Reference yield: 42.0%

2-methoxy-phenol (90-05-1) + ortho-chlorobenzoic acid (118-91-2) → 2-carboxy-2'-methoxydiphenyl ether (21905-73-7)

Guidance literature:

With copper(I) oxide; sodium methylate; at 180 ℃;

DOI:10.1002/ardp.19933260805

Reference yield:

2-methoxy-phenol (90-05-1) + 2-bromobenzoic-acid (88-65-3) → 2-carboxy-2'-methoxydiphenyl ether (21905-73-7)

Guidance literature:

2-methoxy-phenol; 2-bromobenzoic-acid; With caesium carbonate; tetrakis(actonitrile)copper(I) hexafluorophosphate; In toluene; for 15h; Heating / reflux;

With hydrogenchloride; In water; ethyl acetate; toluene;

upstream raw materials:

2-methoxy-2'-methyldiphenyl ether

2-(2-methoxyphenoxy)benzaldehyde

2-methoxy-phenol

ortho-chlorobenzoic acid

Downstream raw materials:

4-hydroxy-9H-xanthen-9-one

4-methoxy-9H-xanthen-9-one

2-(2-hydroxy-phenoxy)-benzoic acid

Guaiaspir

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