2,3-dihydro-4-(2-propen-1-yl)-5-Benzofuranol

Base Information

Chemical Name:2,3-dihydro-4-(2-propen-1-yl)-5-Benzofuranol
CAS No.:119795-45-8
Molecular Formula:C₁₁H₁₂O₂
Molecular Weight:0
Hs Code.:
Mol file:119795-45-8.mol

Synonyms:2,3-dihydro-4-(2-propen-1-yl)-5-Benzofuranol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-dihydro-4-(2-propen-1-yl)-5-Benzofuranol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 2,3-dihydro-4-(2-propen-1-yl)-5-Benzofuranol

There total 1 articles about 2,3-dihydro-4-(2-propen-1-yl)-5-Benzofuranol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.0%

: 119795-46-9
2,3-Dihydro-5-benzofuranyl allyl ether

: 40492-52-2
2,3-dihydrobenzofuran-5-ol

: 119794-84-2
6-allyl-2,3-dihydrobenzofuran-5-ol

: 119795-45-8
4-allyl-2,3-dihydrobenzofuran-5-ol

Guidance literature:: With boron trichloride; In dichloromethane; for 2h; -20 deg to r.t.;
DOI:10.1021/jm00125a014

Reference yield: 56.0%

: 119795-45-8
4-allyl-2,3-dihydrobenzofuran-5-ol

: 108-98-5
thiophenol

: 2,3-Dihydro-4-(3-thiophenoxypropyl)-5-benzofuranol

Guidance literature:: With 2,2'-azobis(isobutyronitrile); at 90 ℃; for 8h;
DOI:10.1021/jm00125a014

Reference yield:

: 119795-45-8
4-allyl-2,3-dihydrobenzofuran-5-ol

: 2,3-dihydro-4-(3-phenoxypropyl)-5-benzofuranol

Guidance literature:: Multi-step reaction with 5 steps

1: 1) BH₃*Me₂S, 2) 2.5N NaOH, 30percent H₂O₂ / 1) Et₂O, r.t., 1 h, 2) abs. EtOH, 25-30 deg C, 30 min

2: 1) NaH / 1) THF, ice bath, 2) r.t., overnight

3: 66 percent / pyridine / 1 h / Ambient temperature

4: dimethylformamide / 80 °C

5: H₂ / 10percent Pd/C / ethanol / 760 Torr

With pyridine; sodium hydroxide; dimethylsulfide borane complex; hydrogen; dihydrogen peroxide; sodium hydride; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00125a014