2-(4-methoxy-3-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

• Chemical Name: 2-(4-methoxy-3-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
• CAS No.: 214360-63-1
• Molecular Formula: C14H21BO3
• Molecular Weight: 248.13
• Mol file: 214360-63-1.mol

Synonyms:2-(4-methoxy-3-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Chemical Property of 2-(4-methoxy-3-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Chemical Property:

• PSA: 27.69000
• LogP: 2.30280
• Storage Temp.: 2-8°C

Purity/Quality:

99% ^*data from raw suppliers

2-(4-Methoxy-3-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(4-methoxy-3-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 5 articles about 2-(4-methoxy-3-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

2-methyl-4-bromoanisole (14804-31-0) + bis(pinacol)diborane (73183-34-3) → 2-(3-Methyl-4-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (214360-63-1)

Guidance literature:

2-methyl-4-bromoanisole; bis(pinacol)diborane; With potassium acetate; In dimethyl sulfoxide; for 0.166667h;

dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In dimethyl sulfoxide; at 80 ℃; for 24h;

Reference yield:

1-iodo-4-methoxy-3-methylbenzene (75581-11-2) + 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane (25015-63-8) → 2-(3-Methyl-4-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (214360-63-1)

Guidance literature:

With triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; at 80 ℃; for 18h;

1-iodo-4-methoxy-3-methylbenzene; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In 1,4-dioxane; at 80 ℃; for 18h;

Reference yield:

2,3-dimethyl-2,3-butane diol (76-09-5) + 3-methyl-4-methoxyphenyl-N,N-diisopropylaminoborane → 2-(3-Methyl-4-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (214360-63-1)

Guidance literature:

3-methyl-4-methoxyphenyl-N,N-diisopropylaminoborane; With methanol; In ethyl acetate; at -5 - 20 ℃; for 1h; Inert atmosphere; Schlenk technique;

2,3-dimethyl-2,3-butane diol; In diethyl ether; at 20 ℃; for 4h; Inert atmosphere; Schlenk technique;

DOI:10.1002/chem.201304861

upstream raw materials:

1-iodo-4-methoxy-3-methylbenzene

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

2-methyl-4-bromoanisole

bis(pinacol)diborane

Downstream raw materials:

7-chloro-3-(2-chloro-4-fluorobenzyl)-5-(4-methoxy-3-methylphenyl)-1-(4-methoxybenzyl)-1H-benzo[e][1,4]diazepin-2(3H)-one

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