4,4'-Bis(N-methyl-N-benzylamino)diphenylmethane

Base Information

Chemical Name:4,4'-Bis(N-methyl-N-benzylamino)diphenylmethane
CAS No.:56383-78-9
Molecular Formula:C29H30N2
Molecular Weight:406.56
Hs Code.:
Mol file:56383-78-9.mol

Synonyms:4,4'-Bis(N-methyl-N-benzylamino)diphenylmethane;4,4'-Methylenebis(N-methyl-N-benzylbenzenamine)

Suppliers and Price of 4,4'-Bis(N-methyl-N-benzylamino)diphenylmethane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 4,4'-Bis(N-methyl-N-benzylamino)diphenylmethane

Chemical Property:

PSA：6.48000
LogP:6.55020

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4,4'-Bis(N-methyl-N-benzylamino)diphenylmethane

There total 4 articles about 4,4'-Bis(N-methyl-N-benzylamino)diphenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 4,4'-bis(methylbenzylamino)diphenylcarbenium perchlorate

: 56383-78-9
4,4'-methylenebis(N-benzyl-N-methylaniline)

: C₂₉H₂₈N₂⁽²⁺⁾*2ClO₄^(1-)

Guidance literature:: In acetonitrile; at 110 - 135 ℃; for 0.416667h;

Reference yield: 93.0%

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: 614-30-2
N-methyl-N-phenyl-benzenemethanamine

: 56383-78-9
4,4'-methylenebis(N-benzyl-N-methylaniline)

Guidance literature:: With copper dichloride; In 2,4-dichlorophenoxyacetic acid dimethylamine; at 140 ℃; for 10h;
DOI:10.1039/c2cc32009f

Reference yield:

: 100-39-0
benzyl bromide

: 100-61-8
N-methylaniline

: 56383-78-9
4,4'-methylenebis(N-benzyl-N-methylaniline)

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / dimethyl sulfoxide / 20 - 50 °C

2: copper dichloride / 2,4-dichlorophenoxyacetic acid dimethylamine / 10 h / 140 °C

With potassium hydroxide; copper dichloride; In 2,4-dichlorophenoxyacetic acid dimethylamine; dimethyl sulfoxide;
DOI:10.1039/c2cc32009f