2-Phenyl-5,6-dihydrobenzo[d]thiazol-7(4H)-one

Base Information

Chemical Name:2-Phenyl-5,6-dihydrobenzo[d]thiazol-7(4H)-one
CAS No.:17583-15-2
Molecular Formula:C13H11NOS
Molecular Weight:229.302
Hs Code.:2934200090
DSSTox Substance ID:DTXSID30509011
Wikidata:Q82366309
Mol file:17583-15-2.mol

Synonyms:17583-15-2;2-Phenyl-5,6-dihydrobenzo[d]thiazol-7(4H)-one;2-phenyl-4,5,6,7-tetrahydro-1,3-benzothiazol-7-one;2-phenyl-5,6-dihydro-4H-1,3-benzothiazol-7-one;7(4H)-Benzothiazolone, 5,6-dihydro-2-phenyl-;2-Phenyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;SCHEMBL12965399;DTXSID30509011;AKOS011172042;5,6-dihydro-2-phenyl-7(4h)benzothiazolone;CS-0216783;EN300-60139;Z1245633934

Suppliers and Price of 2-Phenyl-5,6-dihydrobenzo[d]thiazol-7(4H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Phenyl-4,5,6,7-tetrahydro-1,3-benzothiazol-7-one
50mg
$ 90.00

TRC
2-Phenyl-4,5,6,7-tetrahydro-1,3-benzothiazol-7-one
25mg
$ 45.00

Crysdot
2-Phenyl-5,6-dihydrobenzo[d]thiazol-7(4H)-one 95+%
1g
$ 668.00

Chemenu
2-phenyl-5,6-dihydrobenzo[d]thiazol-7(4H)-one 95%
1g
$ 632.00

Alichem
2-Phenyl-5,6-dihydrobenzo[d]thiazol-7(4H)-one
1g
$ 571.20

AK Scientific
2-Phenyl-5,6-dihydrobenzo[d]thiazol-7(4H)-one
2.5g
$ 892.00

Total 7 raw suppliers

Chemical Property of 2-Phenyl-5,6-dihydrobenzo[d]thiazol-7(4H)-one

Chemical Property:

PSA：58.20000
LogP:3.32910
Storage Temp.:2-8°C
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:229.05613515
Heavy Atom Count:16
Complexity:275

Purity/Quality:

99% ^*data from raw suppliers

2-Phenyl-4,5,6,7-tetrahydro-1,3-benzothiazol-7-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2=C(C(=O)C1)SC(=N2)C3=CC=CC=C3

Technology Process of 2-Phenyl-5,6-dihydrobenzo[d]thiazol-7(4H)-one

There total 5 articles about 2-Phenyl-5,6-dihydrobenzo[d]thiazol-7(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: dimethyl <(4,5,6,7-tetrahydro-7-hydroxy-2-phenyl)benzothiazol-7-yl>phosphonate

: 17583-15-2
2-phenyl-5,6-dihydrobenzo[d]thiazol-7(4H)-one

Guidance literature:: With sodium hydroxide; for 0.333333h; Ambient temperature;
DOI:10.1007/BF00817312

Reference yield: 68.0%

: 932-23-0
2-chloro-cyclohexane-1,3-dione

: 2227-79-4
benzenecarbothioamide

: 17583-15-2
2-phenyl-5,6-dihydrobenzo[d]thiazol-7(4H)-one

Guidance literature:: 2-chloro-cyclohexane-1,3-dione; benzenecarbothioamide; In melt; at 140 ℃;

In toluene; for 2h; Dean-Stark; Reflux;

With sodium carbonate; In chloroform; water; at 20 ℃; Solvent;
DOI:10.1080/00397911.2020.1808224

Reference yield:

: 2227-79-4
benzenecarbothioamide

: 17583-15-2
2-phenyl-5,6-dihydrobenzo[d]thiazol-7(4H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / ethanol / 9 h / 80 °C

2: 95 percent / 0.5N NaOH / 0.33 h / Ambient temperature

With sodium hydroxide; In ethanol;
DOI:10.1007/BF00817312