Di-tert-butyl (6-aMino-2-MethylpyriMidin-4-yl)carbaMate

Base Information

Chemical Name:Di-tert-butyl (6-aMino-2-MethylpyriMidin-4-yl)carbaMate
CAS No.:1364663-30-8
Molecular Formula:C15H24N4O4
Molecular Weight:324.38
Hs Code.:2933399990
Mol file:1364663-30-8.mol

Synonyms:Di-tert-butyl (6-aMino-2-MethylpyriMidin-4-yl)carbaMate;2-Methyl-6-[bis(tert-butoxycarbonyl)-amino]-4-aminopyrimidine;tert-Butyl (6-aMino-2-MethylpyriMidin-4-yl)(tert-butyl)carbaMate

Suppliers and Price of Di-tert-butyl (6-aMino-2-MethylpyriMidin-4-yl)carbaMate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
Di-tert-butyl (6-amino-2-methylpyrimidin-4-yl)carbamate
1 g
$ 624.00

Crysdot
tert-Butyl(6-amino-2-methylpyrimidin-4-yl)(tert-butyl)carbamate 95+%
250mg
$ 166.00

Crysdot
tert-Butyl(6-amino-2-methylpyrimidin-4-yl)(tert-butyl)carbamate 95+%
5g
$ 1252.00

Crysdot
tert-Butyl(6-amino-2-methylpyrimidin-4-yl)(tert-butyl)carbamate 95+%
1g
$ 414.00

Chemenu
tert-Butyl(6-amino-2-methylpyrimidin-4-yl)(tert-butyl)carbamate 95%
1g
$ 387.00

Chemenu
tert-Butyl(6-amino-2-methylpyrimidin-4-yl)(tert-butyl)carbamate 95%
5g
$ 1171.00

Alichem
Di-tert-butyl(6-amino-2-methylpyrimidin-4-yl)carbamate
5g
$ 984.87

Total 9 raw suppliers

Chemical Property of Di-tert-butyl (6-aMino-2-MethylpyriMidin-4-yl)carbaMate

Chemical Property:

Boiling Point:436.8±55.0 °C(Predicted)
PKA:5.76±0.10(Predicted)
PSA：107.64000
Density:1.194±0.06 g/cm3(Predicted)
LogP:3.62500

Purity/Quality:

97% ^*data from raw suppliers

Di-tert-butyl (6-amino-2-methylpyrimidin-4-yl)carbamate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Di-tert-butyl (6-aMino-2-MethylpyriMidin-4-yl)carbaMate

There total 4 articles about Di-tert-butyl (6-aMino-2-MethylpyriMidin-4-yl)carbaMate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1365992-81-9
(6-azido-2-methylpyrimidin-4-yl)-bis-carbamic acid tert-butyl ester

: 1364663-30-8
(6-amino-2-methylpyrimidin-4-yl)-bis-carbamic acid tert-butyl ester

Guidance literature:: With hydrogen; 5%-palladium/activated carbon; In industrial methylated spirits; ethyl acetate; at 20 ℃; for 18h;

Reference yield:

: 1749-68-4
4-amino-6-chloro-2-methylpyrimidine

: 1364663-30-8
(6-amino-2-methylpyrimidin-4-yl)-bis-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: dmap / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

2: sodium azide / dimethyl sulfoxide / 16 h / 50 °C

3: hydrogen / 5%-palladium/activated carbon / ethyl acetate; industrial methylated spirits / 18 h / 20 °C

With dmap; sodium azide; hydrogen; 5%-palladium/activated carbon; In tetrahydrofuran; industrial methylated spirits; dimethyl sulfoxide; ethyl acetate;

Reference yield:

: 1350918-95-4
(6-chloro-2-methylpyrimidin-4-yl)-bis-carbamic acid tert-butylester

: 1364663-30-8
(6-amino-2-methylpyrimidin-4-yl)-bis-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / dimethyl sulfoxide / 16 h / 50 °C

2: hydrogen / 5%-palladium/activated carbon / ethyl acetate; industrial methylated spirits / 18 h / 20 °C

With sodium azide; hydrogen; 5%-palladium/activated carbon; In industrial methylated spirits; dimethyl sulfoxide; ethyl acetate;