2-Acetylamino-1-O,3-O,4-O,6-O-tetrakis(trimethylsilyl)-2-deoxy-α-D-glucopyranose

Base Information

Chemical Name:2-Acetylamino-1-O,3-O,4-O,6-O-tetrakis(trimethylsilyl)-2-deoxy-α-D-glucopyranose
CAS No.:53110-68-2
Molecular Formula:C20H47NO6Si4
Molecular Weight:509.93
Hs Code.:
Mol file:53110-68-2.mol

Synonyms:N-((2R,3R,4R,5R,6R)-2,4,5-Tris-trimethylsilanyloxy-6-trimethylsilanyloxymethyl-tetrahydro-pyran-3-yl)-acetamide;2-Acetamido-2-desoxy-tetrakis-O-trimethylsilyl-α-D-glucose;Per-O-trimethylsilyl-2-acetamido-2-deoxy-α-D-glucopyranose;

Suppliers and Price of 2-Acetylamino-1-O,3-O,4-O,6-O-tetrakis(trimethylsilyl)-2-deoxy-α-D-glucopyranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 2-Acetylamino-1-O,3-O,4-O,6-O-tetrakis(trimethylsilyl)-2-deoxy-α-D-glucopyranose

Chemical Property:

PSA：75.25000
LogP:4.75010

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Acetylamino-1-O,3-O,4-O,6-O-tetrakis(trimethylsilyl)-2-deoxy-α-D-glucopyranose

There total 4 articles about 2-Acetylamino-1-O,3-O,4-O,6-O-tetrakis(trimethylsilyl)-2-deoxy-α-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 925673-04-7
2-amino-2-deoxy-1,3,4,6-tetra-O-(trimethylsilyl)-α-D-glucopyranose

: 108-24-7
acetic anhydride

: 53110-68-2
2-acetamido-2-deoxy-1,3,4,6-tetra-O-trimethylsilyl-α-D-glucopyranose

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c4cc06645f

Reference yield:

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 53110-68-2
2-acetamido-2-deoxy-1,3,4,6-tetra-O-trimethylsilyl-α-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 3 h / 20 °C / Inert atmosphere

2: pyridine / dichloromethane / 2 h / 0 °C / Inert atmosphere

With pyridine; In dichloromethane; acetonitrile;
DOI:10.1039/c4cc06645f

Reference yield:

: 90-76-6,90-77-7,530-23-4,579-32-8,579-33-9,643-68-5,2596-19-2,6490-68-2,6490-70-6,6490-72-8,6490-73-9,6490-74-0,14196-84-0,14196-86-2,14257-69-3,58381-21-8
glucosamine

: 53110-68-2
2-acetamido-2-deoxy-1,3,4,6-tetra-O-trimethylsilyl-α-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 3 h / 20 °C / Inert atmosphere

2: pyridine / dichloromethane / 2 h / 0 °C / Inert atmosphere

With pyridine; In dichloromethane; acetonitrile;
DOI:10.1039/c4cc06645f