D-Glucuronal 3,4-Diacetate Methyl Ester

Base Information

Chemical Name:D-Glucuronal 3,4-Diacetate Methyl Ester
CAS No.:34296-99-6
Molecular Formula:C11H14O7
Molecular Weight:258.228
Hs Code.:
Mol file:34296-99-6.mol

Synonyms:D-Glucuronal 3,4-Diacetate Methyl Ester;1,2-Dideoxy-D-lyxo-Hex-1-enopyranuronic Acid Diacetate Methyl Ester;2,6-Anhydro-5-deoxy-D-arabino-Hex-5-enonic Acid Diacetate Methyl Ester

Suppliers and Price of D-Glucuronal 3,4-Diacetate Methyl Ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
D-Glucuronal 3,4-Diacetate Methyl Ester
10mg
$ 460.00

TRC
D-Glucuronal3,4-DiacetateMethylEster
25mg
$ 165.00

Biosynth Carbosynth
3,4-Di-O-acetyl-D-glucuronal methyl ester
100 mg
$ 1638.00

Biosynth Carbosynth
3,4-Di-O-acetyl-D-glucuronal methyl ester
50 mg
$ 901.00

Biosynth Carbosynth
3,4-Di-O-acetyl-D-glucuronal methyl ester
25 mg
$ 496.00

Biosynth Carbosynth
3,4-Di-O-acetyl-D-glucuronal methyl ester
10 mg
$ 272.60

Biosynth Carbosynth
3,4-Di-O-acetyl-D-glucuronal methyl ester
5 mg
$ 150.00

Total 4 raw suppliers

Chemical Property of D-Glucuronal 3,4-Diacetate Methyl Ester

Chemical Property:

PSA：88.13000
LogP:-0.06470
Solubility.:Chloroform, Dichloromethane, Ethyl Acetate

Purity/Quality:

97% ^*data from raw suppliers

D-Glucuronal 3,4-Diacetate Methyl Ester ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses D-Glucuronal 3,4-Diacetate Methyl Ester (cas# 34296-99-6) is a compound useful in organic synthesis.

Technology Process of D-Glucuronal 3,4-Diacetate Methyl Ester

There total 1 articles about D-Glucuronal 3,4-Diacetate Methyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 15910-11-9
1,4-diacetoxy 1,3-butadiene

: 922-68-9
Methyl glyoxylate

: 34296-99-6,57690-62-7,77942-61-1,95530-81-7,95530-82-8
methyl 3,4-di-O-acetyl-DL-xylo-hex-1-enopyranuronate

: 77824-27-2,77824-28-3
methyl 1,4-di-O-acetyl-2,3-dideoxy-α-DL-erythro-hex-2-enopyranuronate

: 77824-27-2,77824-28-3
methyl 1,4-di-O-acetyl-2,3-dideoxy-α-DL-threo-hex-2-enopyranuronate

Guidance literature:: With hydroquinone; In benzene; at 125 ℃; for 60h;
DOI:10.1016/S0008-6215(00)85239-8

Reference yield:

: 34296-99-6
methyl 3,4-di-O-acetyl-2,6-anhydro-5-deoxy-D-arabino-hex-5-enonate

: 4713-64-8,90319-06-5
2-acetamido-2-deoxy-D-galactopyranosyluronic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) sodium azide, ceric ammonium nitrate / 1.) acetonitrile, -15 deg C, 16 h, 2.) glacial acetic acid, 100 deg C, 1.5 h

2: 4M hydrochloric acid / H₂O / 1.) 40 deg C, 2.) room temperature, 3 h

3: hydrogen / 10percent palladium-on-charcoal / methanol / Ambient temperature

4: methanol / Ambient temperature

With hydrogenchloride; sodium azide; ammonium cerium(IV) nitrate; hydrogen; palladium on activated charcoal; In methanol; water;
DOI:10.1016/S0008-6215(82)80021-9

Reference yield:

: 127-09-3
sodium acetate

: 34296-99-6
methyl 3,4-di-O-acetyl-2,6-anhydro-5-deoxy-D-arabino-hex-5-enonate

: 81997-92-4
methyl 1,3,4-tri-O-acetyl-2-azido-2-deoxy-α-D-galacturonate

Guidance literature:: With sodium azide; ammonium cerium(IV) nitrate; Yield given. Multistep reaction; 1.) acetonitrile, -15 deg C, 16 h, 2.) glacial acetic acid, 100 deg C, 1.5 h;
DOI:10.1016/S0008-6215(82)80021-9