3-Chloro-2,4-dibromo-6-methoxyaniline

Base Information

• Chemical Name: 3-Chloro-2,4-dibromo-6-methoxyaniline
• CAS No.: 860586-90-9
• Molecular Formula: C7H6Br2ClNO
• Molecular Weight: 315.392
• Hs Code.: 2922299090
• Mol file: 860586-90-9.mol

Synonyms:3-Chloro-2,4-dibromo-6-methoxyaniline

Chemical Property of 3-Chloro-2,4-dibromo-6-methoxyaniline

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 112-113°C
• Boiling Point: 327.856°C at 760 mmHg
• Flash Point: 152.082°C
• PSA: 35.25000
• Density: 1.971g/cm³
• LogP: 4.03700

Purity/Quality:

98% ^*data from raw suppliers

2,4-Dibromo-3-chloro-6-methoxyaniline 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Chloro-2,4-dibromo-6-methoxyaniline

There total 5 articles about 3-Chloro-2,4-dibromo-6-methoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

5-chloro-2-methoxyaniline (95-03-4) → 2,4-dibromo-3-chloro-6-methoxyaniline (860586-90-9)

Guidance literature:

With N-Bromosuccinimide; In N,N-dimethyl-formamide; for 1h; Cooling with ice;

Reference yield:

4-chloromethoxybenzene (623-12-1) → 2,4-dibromo-3-chloro-6-methoxyaniline (860586-90-9)

Guidance literature:

Multi-step reaction with 3 steps

1: nitric acid

2: tin; concentrated hydrochloric acid

3: glacial acetic acid; bromine / unter Kuehlung

With hydrogenchloride; tin; bromine; nitric acid; acetic acid;

DOI:10.1017/S1092852900017430

Reference yield:

4-chloro-2-nitroanisole (89-21-4) → 2,4-dibromo-3-chloro-6-methoxyaniline (860586-90-9)

Guidance literature:

Multi-step reaction with 2 steps

1: tin; concentrated hydrochloric acid

2: glacial acetic acid; bromine / unter Kuehlung

With hydrogenchloride; tin; bromine; acetic acid;

DOI:10.1017/S1092852900017430

upstream raw materials:

5-chloro-2-methoxyaniline

bromine

acetic acid

4-chloromethoxybenzene

Downstream raw materials:

3,5-dibromo-4-chloro-2,6-dinitro-anisole

2,6-dibromo-4-chlorophenol

1,3-dibromo-2-chloro-5-methoxybenzene