2,2',4-Trihydroxy-4'-methoxy-6,6'-dimethylbenzophenone

Base Information

Chemical Name:2,2',4-Trihydroxy-4'-methoxy-6,6'-dimethylbenzophenone
CAS No.:21147-34-2
Molecular Formula:C₁₆H₁₆O₅
Molecular Weight:288.3
Hs Code.:2914509090
Mol file:21147-34-2.mol

Synonyms:2,2',4-Trihydroxy-4'-methoxy-6,6'-dimethylbenzophenone

Suppliers and Price of 2,2',4-Trihydroxy-4'-methoxy-6,6'-dimethylbenzophenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2,2',4-Trihydroxy-4'-methoxy-6,6'-dimethylbenzophenone

Chemical Property:

PSA：86.99000
LogP:2.65980

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,2',4-Trihydroxy-4'-methoxy-6,6'-dimethylbenzophenone

There total 5 articles about 2,2',4-Trihydroxy-4'-methoxy-6,6'-dimethylbenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78135-71-4
2,2',4'-tribenzyl-4-methoxy-6,6'-dimethylbenzophenone

: 21147-34-2
2,2',4'-trihydroxy-4-methoxy-6,6'-dimethylbenzophenone

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethyl acetate;
DOI:10.1039/P19810000855

Reference yield:

: 520-43-4
2-hydroxy-4-methoxy-6-methyl-benzoic acid methyl ester

: 21147-34-2
2,2',4'-trihydroxy-4-methoxy-6,6'-dimethylbenzophenone

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / acetone / 20 h / Heating

2: 17.1 g / KOH (aq) / dimethylsulfoxide / 6 h / Heating

3: 95 percent / trifluoroacetic anhydride / 1,2-dichloro-ethane / room temperature -> reflux

4: H₂, HCl (conc) / Pd-C / ethyl acetate

With hydrogenchloride; potassium hydroxide; hydrogen; potassium carbonate; trifluoroacetic anhydride; palladium on activated charcoal; In dimethyl sulfoxide; ethyl acetate; 1,2-dichloro-ethane; acetone;
DOI:10.1039/P19810000855

Reference yield:

: 3187-58-4
methyl orsellinate

: 21147-34-2
2,2',4'-trihydroxy-4-methoxy-6,6'-dimethylbenzophenone

Guidance literature:: Multi-step reaction with 5 steps

1: 23.0 g / K₂CO₃ / acetone / 20 h / Heating

2: K₂CO₃ / acetone / 20 h / Heating

3: 17.1 g / KOH (aq) / dimethylsulfoxide / 6 h / Heating

4: 95 percent / trifluoroacetic anhydride / 1,2-dichloro-ethane / room temperature -> reflux

5: H₂, HCl (conc) / Pd-C / ethyl acetate

With hydrogenchloride; potassium hydroxide; hydrogen; potassium carbonate; trifluoroacetic anhydride; palladium on activated charcoal; In dimethyl sulfoxide; ethyl acetate; 1,2-dichloro-ethane; acetone;
DOI:10.1039/P19810000855