(2-FORMYL-4-METHOXY-PHENOXY)-ACETONITRILE

Base Information

• Chemical Name: (2-FORMYL-4-METHOXY-PHENOXY)-ACETONITRILE
• CAS No.: 149384-09-8
• Molecular Formula: C10H9NO3
• Molecular Weight: 191.18
• Hs Code.: 2926909090
• Mol file: 149384-09-8.mol

Synonyms:(2-FORMYL-4-METHOXY-PHENOXY)-ACETONITRILE;2-(2-FORMYL-4-METHOXYPHENOXY)ACETONITRILE

Chemical Property of (2-FORMYL-4-METHOXY-PHENOXY)-ACETONITRILE

Chemical Property:

• Melting Point: 68-69°
• Boiling Point: 380.9±27.0 °C(Predicted)
• PSA: 59.32000
• Density: 1.202±0.06 g/cm3(Predicted)
• LogP: 1.41008

Purity/Quality:

98%min ^*data from raw suppliers

2-(2-formyl-4-methoxyphenoxy)acetonitrile ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2-FORMYL-4-METHOXY-PHENOXY)-ACETONITRILE

There total 2 articles about (2-FORMYL-4-METHOXY-PHENOXY)-ACETONITRILE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-hydroxy-5-methoxybenzaldehyde (672-13-9) + cyanomethyl bromide (590-17-0) → 2-(2-formyl-4-methoxyphenoxy)acetonitrile (149384-09-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 8h;

DOI:10.1021/jo501328

Reference yield:

2-hydroxy-5-methoxybenzaldehyde (672-13-9) + chloroacetonitrile (107-14-2) → 2-(2-formyl-4-methoxyphenoxy)acetonitrile (149384-09-8)

Guidance literature:

With potassium iodide; potassium carbonate; In N,N-dimethyl-formamide;

Reference yield:

2-(2-formyl-4-methoxyphenoxy)acetonitrile (149384-09-8) + benzenesufonyl hydrazide (80-17-1) → C16H15N3O4S

Guidance literature:

With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 3h;

DOI:10.1021/jo501328

upstream raw materials:

2-hydroxy-5-methoxybenzaldehyde

chloroacetonitrile

cyanomethyl bromide

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